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|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
ab90d632003152d00089bddb8ec99cf1187bc9b77b3f3d426fdba3c72fa1663d | 149ff4f06553e30370ce225adf552f349d99d038be2823415c9b8e4133dcf664 | fsri | data/runs/2026-10-30_thermal/raw/07881edda6af36735b0d0bcd9bd2c357a07de6456f6a4b2633ad1363d615c389.csv | 07881edda6af36735b0d0bcd9bd2c357a07de6456f6a4b2633ad1363d615c389 | LDPE_STA_N2_10KData_210903_R1 | sta_mass_percent | Mass(subtr.2)/% | 103.2231 | % | 103.2231 | % | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/LDPE/STA/N2/10K_min/LDPE_STA_N2_10KData_210903_R1.csv | null | null | null | LDPE_STA_N2_10KData_210903_R1.csv:CSV row 1804 | Mass(subtr.2)/% | fsri_sta_native_csv | separator-v32 | null | null | LDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "LDPE_STA_N2_10KData_210903_R1.csv:CSV row 1804", "source_file": "data/runs/2026-10-30_thermal/raw/07881edda6af36735b0d0bcd9bd2c357a07de6456f6a4b2633ad1363d615c389.csv", "source_sha256": "07881edda6af36735b0d0bcd9bd... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 229.985 | measurement | null | 10 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R1 | fsri:STA:LDPE_STA_N2_10KData_210903_R1 | null | null | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 6... | null | fsri:STA:LDPE_STA_N2_10KData_210903_R1:row:1804:sta_mass_percent | License/reuse permission not established; local research evidence only | 000592d904dc5244959a916e073472fec1166710bf70085f517759a49a246080 | 1 | LDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "LDPE", "labels": ["LDPE"]}, {"field": "sample_id", "text": "LDPE_STA_N2_10KData_210903_R1", "labels": ["LDPE"]}] | LDPE | ||
9225efce5be94c5468463ccaec770c4a47cabc41472ff585ed40ff43dd424cf1 | 22ddd0208c98016632f1f1853700e01d3f8bf9929a4aac30989292b9dd068192 | patents | data/raw/fbd7a8cc6a1501508f28a0345df6b66572f450ef206a06a4cbee372f42b86f35.bin | fbd7a8cc6a1501508f28a0345df6b66572f450ef206a06a4cbee372f42b86f35 | US8252450B2:Com. Ex. 4 | porosity | Porosity (%) | 40 | % | 40 | % | https://patents.google.com/patent/US8252450B2/en | null | TABLE 1 | null | 166 | 3 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "num:p-0167", "text": "Dry-blended were 100 parts by mass of a first polyethylene composition comprising 30% by mass of ultra-high-molecular-weight polyethylene (UHMWPE) having a weight-average molecular weight (Mw) of 2.0×10 6 , and 70% by mass of high-density polyethylene (HDPE) having Mw of 3.5×10 5 and... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0231 | (4) Porosity (%) Measured by a weight method. | null | measured | null | null | null | null | null | accepted | Publication US8252450B2; Com. Ex. 4; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 38581278 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 19238b5b03e4e61c7d0eb9e721f7959861d04e86988ae20488457d4250d1ab07; current SHA256 identifies sanitized bytes. | 0008eb988d12c702a177747b7503fa7c5987cf20113669e8d1abda5509f4e3d4 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
3a96cff29dcc12a95ff60be529917d61f8af5a141f04a544f58303ce72103597 | e965da868152ddda435361a07977cd706b6cbc4ce47b1a2d00bdc2a572461fac | patents | data/raw/a97d94c9bd51368e0ac332fd1b0dd113dc50deb2232cc210dd442264c9c5e144.bin | a97d94c9bd51368e0ac332fd1b0dd113dc50deb2232cc210dd442264c9c5e144 | US6666969B1:Comparative Example 1 | air_permeability_time | Air permeability (sec/100 cc) | 650 | sec/100 cc | 650 | s | https://patents.google.com/patent/US6666969B1/en | null | TABLE 1 | null | 16 | 4 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "css:html:nth-of-type(1) > body:nth-of-type(1) > search-app:nth-of-type(1) > article:nth-of-type(1) > section:nth-of-type(6) > div:nth-of-type(1) > div:nth-of-type(1) > div:nth-of-type(64)", "text": "A polyethylene composition (melting point: 135° C., crystal dispersion temperature: 90° C.) having an Mw/Mn... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | null | (3) Air permeability: Measured according to JIS P8117. | null | measured | null | null | null | {"canonical_unit": "s", "unit_alias": "sec/100 cc"} | null | accepted | Publication US6666969B1; Comparative Example 1; printed unit: sec/100 cc. Example identity and experimental protocol retained; no processing temperature inferred. | 26559929 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 83702f3f6902ccd258fa2e1e1894a7fce70e42caf9852ee9d16b28384034d6a0; current SHA256 identifies sanitized bytes. | 000c7fd3cfe7a21fa5c63802d372aa3dc54e2f6a82d92e5f6df67555392084ee | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
e55a541238c69a1431c11574559ddaade0f2cee1379d0b59cdf123dc1db35221 | 6bdd4097df2398d4d3685eee69fd2e9f8737f1b090e796957a240be061fd0537 | manual | data/runs/2026-10-23_balanced_verified/raw/9b679ede4a6d26bd04ac0a85965559b2ab15cf0b546afc9f54f0197ede120b73.csv | 9b679ede4a6d26bd04ac0a85965559b2ab15cf0b546afc9f54f0197ede120b73 | US20230282933A1:A:Comparative Example 6 | pore_size | Average long pore diameter in ND-MD cross-section | 85 | nm | 0.085 | um | https://patents.google.com/patent/US20230282933A1/en | null | TABLE 4 | null | 79 | 8 | manual_structured_import | separator-v32 | null | null | PP | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "TABLE 4", "source_file": "data/runs/2026-10-23_balanced_verified/raw/9b679ede4a6d26bd04ac0a85965559b2ab15cf0b546afc9f54f0197ede120b73.csv", "source_sha256": "9b679ede4a6d26bd04ac0a85965559b2ab15cf0b546afc9f54f0197e... | Material supplied by source adapter or reviewed import; see source coordinates and notes | single-layer PP | null | null | null | separator | not_reported | null | null | null | mean | null | unknown | null | null | cross-section ND-MD | Reviewed primary experimental geometry tables | Reported membrane thickness/porosity or directional long pore diameter; pore diameter is not a circular-equivalent diameter. Resin density, processing shrinkage and thickness-normalized permeability/strength are excluded. Numeric measurement temperature not reported. | null | measured | null | null | null | {"offset": 0, "scale": 0.001} | null | accepted | Primary SHA256 8fbd97b81341d5262d420aa2b4151eb7a2cb16f8adaed86074da4ff33a81e0af; expanded row 37, column 8; exact label Average long pore diameter in ND-MD cross-section; raw unit nm; printed scalar 85; sample group A. | null | null | Reviewed source-explicit PP/PE/PP whole membrane and component geometry; preserve primary coordinates and scope; normalized mechanical/transport metrics excluded. | 001410a7790a02a22ae1e06714bf080d5317219587ea453ff99b3679190927e4 | 1 | not_reported_in_linked_identity | |||||
6eb063e789cd8f6fd95a5d349ee6f173bfd65eaa0b93373ed4439a7cad765350 | 15b1542a939e3e9dcbed2f999f31a7eb980bc0e5963aaba988b7a6dac2e695db | patents | data/raw/72158dcf1092936d49182d947b2596d87b4ee0e59c54a59bc77e9dec5a904c8b.bin | 72158dcf1092936d49182d947b2596d87b4ee0e59c54a59bc77e9dec5a904c8b | US20100151310A1:Example 5 | porosity | Porosity (%) | 37.9 | % | 37.9 | % | https://patents.google.com/patent/US20100151310A1/en | null | TABLE 1 | null | 85 | 3 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p-0120", "text": "Dry-blended were 100 parts by mass of a polyethylene composition comprising 5% by mass of ultra-high-molecular-weight polyethylene (UHMWPE) having Mw of 1.5×10 6 and Mw/Mn of 8, and 95% by mass of high-density polyethylene (HDPE) having Mw of 3.0×10 5 and Mw/Mn of 8.6, with 0.375 parts b... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0141 | (3) Porosity (%) It was measured by a mass method. | null | measured | null | null | null | null | null | accepted | Publication US20100151310A1; Example 5; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 37708827 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 b27a970562a779fb3be4f7a6886c0db3503e285d7743adc95619eec289f4b842; current SHA256 identifies sanitized bytes. | 001520c3845dcff95bbae97b803db4104f82eda4acb4487814a9c6d7ad8d01aa | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
853acf8ca744ae43bf1a1dd35773f06bbe0ea2c48cc4cd52423b2d107265d7a3 | 741ae90c6257a05dd17eb987c7a386d5c9b574ad61946f9b23c9bead0fa18b75 | patents | data/runs/2026-10-26_balanced/raw/302f2930a6c93c7cb1377cc16d072f6de2d6935752bb7c3f14f4dacb26560d2c.bin | 302f2930a6c93c7cb1377cc16d072f6de2d6935752bb7c3f14f4dacb26560d2c | US20120028131A1:Ex. 10 | shutdown_temperature | Shutdown Temperature (° C.) | 129.1 | ° C. | 129.1 | C | https://patents.google.com/patent/US20120028131A1/en | null | TABLE 1 | null | 41 | 11 | patent_html_table | separator-v32 | null | null | PE | explicit_composition_table | [{"locator": "TABLE-US-00001", "text": "TABLE 1 No. Ex. 1 Ex. 2 Ex. 3 Ex. 4 Ex. 5 Ex. 6 Ex. 7 Ex. 8 Ex. 9 Ex. 10 Resin Composition PE Composition UHMWPE Mw (1) 1.95 × 10 6 1.95 × 10 6 1.95 × 10 6 1.95 × 10 6 1.95 × 10 6 1.95 × 10 6 1.95 × 10 6 1.95 × 10 6 1.95 × 10 6 1.95 × 10 6 % by mass 18 18 18 18 18 18 18 18 18 18 ... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0023 | (d) Shutdown Temperature <130.5° C. The microporous membrane's shutdown temperature is measured by the method disclosed in PCT Patent Publication No. WO2007/052663, which is incorporated by reference herein in its entirety. According to this method, the microporous membrane is exposed to an increasing temperature (5° C... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0 C."} | null | accepted | Publication US20120028131A1; Ex. 10; printed unit: ° C.. Example identity and experimental protocol retained; no processing temperature inferred. | 42828625 | null | License/reuse permission not established; local research evidence only | 001530f296107d712fdfa94c925dd74415b92e6b6ec94be315e72a26e3be02a4 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
db8d6a30b704dc3012ccc1428b411ea72164232de76052786cdfa6b098783ec1 | c555e58813abf95dd64fa18cc2b0c9b0349ac167a358a767cb1782cef5c1e41c | patents | data/runs/2026-10-23_balanced/raw/3040883f6876a37ffad977713cbd26204c52a718432b427a81d47b70ab3ec4d7.bin | 3040883f6876a37ffad977713cbd26204c52a718432b427a81d47b70ab3ec4d7 | EP4375059A1:Comparative Example 4 | porosity | Physic al proper ties Porosity (%) Porosity (%) Porosity (%) Porosity (%) Porosity (%) | 41 | % | 41 | % | https://patents.google.com/patent/EP4375059A1/en | null | table_3 | null | 26 | 10 | patent_html_table | separator-v32 | null | null | PE/PP | reviewed_sample_link | [{"locator": "p0116", "text": "A raw material obtained by dry-blending 0.2 mass% of tetrakis(methylene-3-(3,5-di-tert-butyl-4-hydroxyphenyl)-propionate)methane as an antioxidant with 100 mass% of a polyolefin composition composed of 70 mass% of ultrahigh molecular weight polyethylene having a weight average molecular w... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h0038 | (2) [Porosity (%)] A polyolefin multilayer microporous membrane was cut into a size of 95 mm × 95 mm, and the volume (cm 3 ) and mass (g) of the cut piece were measured. Based on these measurements and a membrane density (g/cm 3 ), the porosity was calculated using the following formula. Porosity = ((volume - mass/memb... | null | measured | null | null | null | null | null | accepted | Publication EP4375059A1; Comparative Example 4; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p0116 | p0117 | p0118 | p0120 | p0124 | p0125 | p0127 | p0130 | p0131 | p0132 | p0133 | 84979946 | null | License/reuse permission not established; local research evidence only | 001a437c92aa2faecf67a8f62d4c5cdb9b9dd8aa2c462b857fff8a50ca6065f1 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE/isotactic PP | ||||
b0dbadb0ae8ee335c0e282d02935ccf51ba260528d3bde973de7c7d5d71223e0 | 0dea6d581abd14726def4375f67162783f2cf13a7698bac96c0eda96f68e1fbb | patents | data/runs/2026-10-23_balanced/raw/ca3748f4f0a6f12d7edbdacd3123d9599826f0f0ae5f0bfb3990072474fa9dec.bin | ca3748f4f0a6f12d7edbdacd3123d9599826f0f0ae5f0bfb3990072474fa9dec | EP4040589A1:Comp Ex.3 | tensile_strength | Tensile strength (kgf/cm 2 ) | 1310 | kgf/cm 2 | 128.467115 | MPa | https://patents.google.com/patent/EP4040589A1/en | null | table_1 | null | 11 | 9 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p0168", "text": "As a polyolefin porous substrate, a polyethylene porous film (available from Toray, porosity: 45%) having a thickness of 9 µm was prepared."}, {"locator": "p0169", "text": "The polyethylene porous substrate was dipped in the photocurable composition for 30 seconds and removed therefrom, f... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h0037 | (6) Evaluation of Tensile Strength in Machine Direction and Transverse Direction and Change in Tensile Strength in Machine Direction A specimen having a size of 100 mm × 15 mm was prepared. According to ASTM D882, the specimen was drawn in each of the machine direction and the transverse direction at a rate of 50 mm/mi... | null | measured | null | null | null | {"offset": 0, "scale": 0.0980665} | null | accepted | Publication EP4040589A1; Comp Ex.3; printed unit: kgf/cm 2 . Example identity and experimental protocol retained; no processing temperature inferred. | 75849009 | null | License/reuse permission not established; local research evidence only | 0020f5c6e3cc319a14ceabf00c1381c02c270f5cf77feb7b87a6c0c230a90462 | 1 | not_reported_in_linked_identity | |||||
e896287a38c4a1277bd7991cb8cfb24ba3f355d0d07eb07f8fe8613cfe4b0fbf | c0f9c74242c9a4495f5140f2ddf8c0db113fa127ab22cae0f1cdda287a9c7c18 | patents | data/runs/2026-10-23_balanced_temperature/raw/4b8b14942d1d30e42e91bb60c6836baa7c0223a16b4bae5bb3880df82dee9f96.bin | 4b8b14942d1d30e42e91bb60c6836baa7c0223a16b4bae5bb3880df82dee9f96 | US20220411600A1:Comparative Example 11 | puncture_force | Puncture strength | 645 | gf | 6.325289 | N | https://patents.google.com/patent/US20220411600A1/en | null | TABLE 5 | null | 11 | 7 | patent_html_table | separator-v32 | null | null | PE | reviewed_sample_link | [{"locator": "TABLE-US-00010", "text": "TABLE 3-2 Comparative Comparative Comparative Comparative Comparative Membrane-forming conditions Example 7 Example 8 Example 9 Example 10 Example 11 PE (1) PE3 PE8 PE3 PE4 PE11 PE (2) — — PE1 — PE12 PP Mv (10,000) PP1 PP1 PP1 PP1 — Plasticizer — LP LP LP LP LP Starting PE1 wt % ... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 23 | measurement | null | null | unspecified | Patent experimental protocol p-0167 | Using a Handy Compression Tester KES-G5™ by Kato Tech Corp., the PO microporous membrane was anchored with a specimen holder having an opening diameter of 11.3 mm. The center section of the anchored microporous membrane was then subjected to a puncture test using a needle with a tip having a diameter of 1.0 mm and a cu... | null | measured | null | null | null | {"offset": 0, "scale": 0.00980665} | null | accepted | Publication US20220411600A1; Comparative Example 11; printed unit: gf. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: TABLE-US-00010 Reviewed conditions: {"basis": "explicit_measurement_temperature", "metadata": {"temperature_C": 23.0, "temperature_ro... | 74037137 | null | License/reuse permission not established; local research evidence only | 00217b53f5a2a2bf22a475c7c161b6c1b1d6812d2fc382f50cbc4122d4a1aed0 | 1 | not_reported_in_linked_identity | |||||
d0c915c2303da244702939509502320e603e8ea02db992edc4ff9b54911f8dd5 | dceb396a8981b259ec248549d088560a330b7821e63fac67520cd2432273e037 | manual | data/runs/2026-10-26_pdf_verified/raw/73ee191d4c972ae18890eafd105f7bb31d7aedd57d830b1da066b9e70cfc328b.csv | 73ee191d4c972ae18890eafd105f7bb31d7aedd57d830b1da066b9e70cfc328b | US20080118827A1:TABLE 1:Sample 8 | thickness | thickness | 9.8 | um | 9.8 | um | https://patents.google.com/patent/US20080118827A1/en | null | TABLE 1 | null | 10 | 10 | manual_structured_import | separator-v32 | null | null | PE/PP/PE | reviewed_pdf_sample_link | [{"source_file": "data/runs/2026-10-26_pdf/raw/4a8ccc22bfd4009721a60f1b79c72edb276f78dc1ef51ddebffefe10d30572da.pdf", "source_sha256": "4a8ccc22bfd4009721a60f1b79c72edb276f78dc1ef51ddebffefe10d30572da", "page": 5, "locator": "PDF page 5, TABLE 1, sample Sample 8; rendered material and measurement rows inspected", "text... | Material row/experimental material section explicitly matched to this sample in the original PDF | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Reviewed primary PDF TABLE 1; source method retained in notes when specified | Primary PDF page 5, TABLE 1; printed separator property. Numeric test temperature unreported unless a dedicated condition is supplied. | null | measured | null | null | null | null | null | accepted | Primary PDF SHA256 4a8ccc22bfd4009721a60f1b79c72edb276f78dc1ef51ddebffefe10d30572da; PDF page 5; primary table row 11, column 10; original printed cell 9.8 um. Material attribution checked in rendered original PDF, not inferred from title. | null | null | Reviewed primary-source PDF cells; original reuse restrictions apply; raw PDFs retained locally | 00231c31e347f827af70e8b3addf1e8641a4d49bf0bc790b87aa014a42b3a501 | 1 | not_reported_in_linked_identity | |||||
34aecae73112bdffa6d6b51da73665d78c5fdee8c0cb4b9dd1dfc811bc3b73da | 293261c992f887fd407c7246c776f9d6192d561d3ffc44bc671e66834c7cd9f2 | patents | data/raw/94ab98c6665420ca7e2cf5b773370697ef59005b2fcc647a776ecd472cef1ec5.bin | 94ab98c6665420ca7e2cf5b773370697ef59005b2fcc647a776ecd472cef1ec5 | US9455432B2:Ex. 1 | thermal_shrinkage | % TD shrinkage @ 90° C. | 0.3 | % | 0.3 | % | https://patents.google.com/patent/US9455432B2/en | null | TABLE 1 | null | 17 | 2 | patent_html_table | separator-v32 | null | null | PE/PP | reviewed_sample_link | [{"locator": "p-0034", "text": "Various thickness hybrid laminated membranes were prepared by laminating wet process PE and dry process PP of different thicknesses. A two-fold improvement in puncture strength was observed when comparing Example 3 which has a puncture strength of 812 gf compared to CE 2 which has a punc... | null | bilayer | null | null | null | separator | not_reported | null | null | null | reported | 90 | exposure | null | null | TD | Patent experimental protocol p-0040 | Shrinkage is measured at two temperatures by placing a sample in an oven at 105 deg C. for one hour and placing a second sample in an oven at 120 deg C. for one hour. Shrinkage is measured in both machine direction (MD) and transverse direction (TD) and is reported as a % MD shrinkage and % TD shrinkage. | null | measured | null | null | null | null | null | accepted | Publication US9455432B2; Ex. 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p-0034 | p-0035 | 51528443 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 be677e3d6cfd7359f0218cf890c7ac8ba3a15d077766a8d74bba9b70173eb254; current SHA256 identifies sanitized bytes. | 0026e96de5d050277ea6b127b3d909e007b246b5bda3b1dd41de61aa7cf5a64d | 1 | not_reported_in_linked_identity | |||||
c081e0ac9f4cba6b83167833bf9b4a1e8031a224b2601d574e254f2ce5e1a995 | 0d4b4057c02f851bd0e2ea1a5a24b6498c318b16f76eb6d7a88fcf24d63097bf | fsri | data/runs/2026-10-30_thermal/raw/bbad75bb0597b2b432823e172f3d1938725c5f50c32ee9923710842896fdbe1f.csv | bbad75bb0597b2b432823e172f3d1938725c5f50c32ee9923710842896fdbe1f | HDPE_STA_N2_30KData_21109_R1 | sta_mass_change | Mass loss(subtr.2)/mg | -0.04483787 | mg | -0 | kg | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/HDPE/STA/N2/30K_min/HDPE_STA_N2_30KData_21109_R1.csv | null | null | null | HDPE_STA_N2_30KData_21109_R1.csv:CSV row 459 | Mass loss(subtr.2)/mg | fsri_sta_native_csv | separator-v32 | null | null | HDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "HDPE_STA_N2_30KData_21109_R1.csv:CSV row 459", "source_file": "data/runs/2026-10-30_thermal/raw/bbad75bb0597b2b432823e172f3d1938725c5f50c32ee9923710842896fdbe1f.csv", "source_sha256": "bbad75bb0597b2b432823e172f3d1... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 95.021 | measurement | null | 30 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R1 | fsri:STA:HDPE_STA_N2_30KData_21109_R1 | null | {"offset": 0.0, "scale": 1e-06} | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 3... | null | fsri:STA:HDPE_STA_N2_30KData_21109_R1:row:459:sta_mass_change | License/reuse permission not established; local research evidence only | 0027b49e8e9429e1a4c2ad2a64e22b2baa3d85323c5ee85509d53cdcc7c3faa2 | 1 | HDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "HDPE", "labels": ["HDPE"]}, {"field": "sample_id", "text": "HDPE_STA_N2_30KData_21109_R1", "labels": ["HDPE"]}] | HDPE | ||
078dc0cf9fb79894f16fb483f3f5c1304eaf449eaf740f18523de329f2d62a80 | ea9a1d8cc9f7f88cc0559e798402751de157c736a1ab46164a2845c2afeeb8a1 | patents | data/raw/3b4fb8a19b3c1b3c82e8d55e982f602224f6563ba0910b674a0ec6d2eec30336.bin | 3b4fb8a19b3c1b3c82e8d55e982f602224f6563ba0910b674a0ec6d2eec30336 | US20240055722A1:Example 28 | thermal_shrinkage | TD heat shrinkage at 120° C. | 14.5 | % | 14.5 | % | https://patents.google.com/patent/US20240055722A1/en | null | TABLE 7 | null | 31 | 7 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p-0349", "text": "(A) As shown in Table 5, 30 parts by weight of a polyethylene having an My of 900,000 and 70 parts by weight of a polyethylene having an My of 300,000 were dry-blended, and the resultant was further blended with 0.3 parts by weight of tetrakis(methylene-3-(3′,5′-di-t-butyl-4′-hydroxyphen... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 120 | exposure | 60 | null | TD | Patent experimental protocol p-0282 | As a sample, a porous membrane was cut into a piece having a pre-heating length (mm) of 100 mm in the MD and 100 mm in the TD, 50 mm in the MD and 50 mm in the TD, or 30 mm in the MD and 30 mm in the TD, and the thus obtained sample was left to stand in an oven at 120° C. for 1 hour. In this process, the sample was san... | length | measured | null | null | null | null | null | accepted | Publication US20240055722A1; Example 28; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 81382650 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 4405cda9233b1ad50ce58fa0e6aee041740117f0e0e3250cfc2886f0618ce3fb; current SHA256 identifies sanitized bytes. | 0029b05a96d0a55f794097bc5ebed95c29a9c52549589527c40deb96be4e1147 | 1 | not_reported_in_linked_identity | |||||
4fe1e38c66b3c5a5300ac982d2cd382c5290cd165a470fd730a42f4e4018d28f | 639703ae959cdb998aad8516b10f5f4d81578335b5a57192d00634a2cb1827e8 | fsri | data/runs/2026-10-30_thermal/raw/8a6f6ee5c0fd3efc8999d65a90e74a6e4a49b25c7c3e93cf17c8a105de2c01c0.csv | 8a6f6ee5c0fd3efc8999d65a90e74a6e4a49b25c7c3e93cf17c8a105de2c01c0 | HDPE_STA_N2_10KData_21109_R3 | sta_mass_change | Mass loss(subtr.2)/mg | -0.01557726 | mg | -0 | kg | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/HDPE/STA/N2/10K_min/HDPE_STA_N2_10KData_21109_R3.csv | null | null | null | HDPE_STA_N2_10KData_21109_R3.csv:CSV row 2505 | Mass loss(subtr.2)/mg | fsri_sta_native_csv | separator-v32 | null | null | HDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "HDPE_STA_N2_10KData_21109_R3.csv:CSV row 2505", "source_file": "data/runs/2026-10-30_thermal/raw/8a6f6ee5c0fd3efc8999d65a90e74a6e4a49b25c7c3e93cf17c8a105de2c01c0.csv", "source_sha256": "8a6f6ee5c0fd3efc8999d65a90e7... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 300.021 | measurement | null | 10 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R3 | fsri:STA:HDPE_STA_N2_10KData_21109_R3 | null | {"offset": 0.0, "scale": 1e-06} | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 4... | null | fsri:STA:HDPE_STA_N2_10KData_21109_R3:row:2505:sta_mass_change | License/reuse permission not established; local research evidence only | 002f4a88d635be4128a2ccb6f7e7cd50a78837feada0670b650d7bd0b64f7774 | 1 | HDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "HDPE", "labels": ["HDPE"]}, {"field": "sample_id", "text": "HDPE_STA_N2_10KData_21109_R3", "labels": ["HDPE"]}] | HDPE | ||
eecef855e4d5eb2af657b14df5bf06b6a7c8c8ca9238f4fafe9b7d3ed52a994e | 6922f0529fe9fee37986d22cd842cb62f41b0bbf86d45de87f8c733b42ba2c68 | patents | data/runs/2026-10-26_balanced/raw/1ba10a90dcfce0c2d3dc97c62b78399c58259dbbad698b76014deda100a05859.bin | 1ba10a90dcfce0c2d3dc97c62b78399c58259dbbad698b76014deda100a05859 | US20210214535A1:Comparative Example 1 | porosity | properties Porosity (%) | 45 | % | 45 | % | https://patents.google.com/patent/US20210214535A1/en | null | TABLE 3 | null | 7 | 4 | patent_html_table | separator-v32 | null | null | PE/PP | inherited_recipe | [{"locator": "p-0191", "text": "A polyolefin microporous membrane was produced by the following procedures. A composition of the resin raw material contained 70 parts by weight of polyethylene having a melting point of 135° C., viscosity-average molecular weight of 700,000 and molecular weight distribution of 5.0 as th... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0025 | <Porosity (%)> A 10 cm×10 cm square sample was cut out from the microporous membrane, the volume (cm 3 ) and weight (g) of the sample were measured, and the porosity was calculated based on them and the membrane density (g/cm 3 ) according to the following equation: Porosity (%)=(Volume−Weight/Membrane density)/Volume×... | null | measured | null | null | null | null | null | accepted | Publication US20210214535A1; Comparative Example 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 72338531 | null | License/reuse permission not established; local research evidence only | 00320cc8a4491458179f9f403f2c8ca1ad61d4f7f53a6d5752132f3bb6a7e233 | 1 | not_reported_in_linked_identity | isotactic PP | ||||
3ec562721040aef478e9d5f76a3cec97d256f31e195a78ebd47c87b86f43dab4 | ab5d07a8f8e47cd1462c004ec7c39811f1a5e2a70e7a0b51a47e6d3c6d5aaa7c | patents | data/raw/0a8a43a71685068c8d272d5eaed6d6ad158cf59515a876ad50e4e739e44790da.bin | 0a8a43a71685068c8d272d5eaed6d6ad158cf59515a876ad50e4e739e44790da | US20120115008A1:Comparative Example 8 | shutdown_temperature | Shutdown temperature | 146 | ° C. | 146 | C | https://patents.google.com/patent/US20120115008A1/en | null | TABLE 2 | null | 48 | 5 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p-0223", "text": "As a polyethylene powder, GUR2126 (weight-averaged molecular weight: 4,150,000, melting point: 141° C.) and GURX143 (weight-averaged molecular weight: 560,000, melting point: 135° C.) manufactured by Ticona were used. A polyethylene solution was produced by making the mixing ratio of GUR... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0212 | (11) Shutdown Temperature The shutdown temperatures of the polyolefin microporous membrane and the separator for a non-aqueous secondary battery were obtained by the following method. A sample was punched in a circular shape having a diameter of 19 mm and immersed in a methanol solution (methanol: manufactured by Wako ... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0 C."} | null | accepted | Publication US20120115008A1; Comparative Example 8; printed unit: ° C.. Example identity and experimental protocol retained; no processing temperature inferred. | 44673209 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 2f67082b26eb472cc609c03b0999afa775ae991bb61b38d1c4eef1ee2b37c899; current SHA256 identifies sanitized bytes. | 003d0b37b435d472f9d83c6edae58df38bd60a2d2891571e30ad7100dd9a9f9d | 1 | not_reported_in_linked_identity | |||||
ae6abfa5c89c0e065c355c999793e16b51b7b2acd0ca866a85edf056147ad18d | 3297d03f9b6c615033b08b847a151fa041371df5eaaa2da6a69898a32833c47f | fsri | data/runs/2026-10-30_thermal/raw/854c0a11f1d4ea95762124db2ad0a105a0d333c0f54e26b044a3dd27abc8c81d.csv | 854c0a11f1d4ea95762124db2ad0a105a0d333c0f54e26b044a3dd27abc8c81d | LDPE_STA_N2_30KData_210908_R3 | sta_mass_percent | Mass(subtr.2)/% | 99.95924000000001 | % | 99.95924 | % | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/LDPE/STA/N2/30K_min/LDPE_STA_N2_30KData_210908_R3.csv | null | null | null | LDPE_STA_N2_30KData_210908_R3.csv:CSV row 2410 | Mass(subtr.2)/% | fsri_sta_native_csv | separator-v32 | null | null | LDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "LDPE_STA_N2_30KData_210908_R3.csv:CSV row 2410", "source_file": "data/runs/2026-10-30_thermal/raw/854c0a11f1d4ea95762124db2ad0a105a0d333c0f54e26b044a3dd27abc8c81d.csv", "source_sha256": "854c0a11f1d4ea95762124db2ad... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 290.02 | measurement | null | 30 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R3 | fsri:STA:LDPE_STA_N2_30KData_210908_R3 | null | null | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 a... | null | fsri:STA:LDPE_STA_N2_30KData_210908_R3:row:2410:sta_mass_percent | License/reuse permission not established; local research evidence only | 003d994d9881dfaac933bccb3667fd9a70e2d32effaf227b49e443439525a13d | 1 | LDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "LDPE", "labels": ["LDPE"]}, {"field": "sample_id", "text": "LDPE_STA_N2_30KData_210908_R3", "labels": ["LDPE"]}] | LDPE | ||
13c48e87e732338c2a7bf27016c1748348bc2f2dba7b7a26679501a9648e98f9 | 1b603e8af626d51bb377c773c8ddec9d1d48df8753ea6f3fdd3464234c4af086 | patents | data/raw/3b599b269f4a18e8759ca9a8f4c287011da641e1c752d630aa98bfb1567696b4.bin | 3b599b269f4a18e8759ca9a8f4c287011da641e1c752d630aa98bfb1567696b4 | US10680224B2:Comparative Example 5 | pore_size | Maximum pore size nm | 55 | nm | 0.055 | um | https://patents.google.com/patent/US10680224B2/en | null | TABLE 2 | null | 28 | 8 | patent_html_table | separator-v32 | null | null | PE | reviewed_sample_link | [{"locator": "p-0172", "text": "TABLE 2 Comparative Comparative Comparative Comparative Comparative Comparative Comparative Example 1 Example 2 Example 3 Example 4 Example 5 Example 6 Example 7 First UHMwPE Mass % 30 — — — — — 15 layer HDPE 60 40 50 30 — — 75 PP(D) 10 60 50 70 — — 10 Resin/solvent Parts by 30/70 25/75 ... | null | monolayer | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0088 | (4) Maximum Pore Size and Mean Flow Pore Size (Nm) The maximum pore size and mean flow pore size were measured in the order of Dry-up and Wet-up using a perm porometer (CFP-1500A manufactured by PMI). For Wet-up, pressure was applied to a microporous membrane sufficiently immersed in Galwick (trade name) manufactured b... | null | measured | null | null | null | {"offset": 0, "scale": 0.001} | null | accepted | Publication US10680224B2; Comparative Example 5; printed unit: nm. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p-0172 | 54935643 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 37b2324c9c93789bbb48e154f20b2f2777c2e6c80f7dd58cb121f909aa7fc5e8; current SHA256 identifies sanitized bytes. | 004567c8ee2a1d7d3c3f43d5fccbb55ebb1197f5b277eb57f1045145dda5f901 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
03037e6b9d4897c1fe5f4abce7afabfec845448eeca9153a235eb3e95c658482 | 1fa216de896c40bf4ffabec9737a7663b5faef676f09837ed5f8a0a057a59573 | patents | data/raw/3cb9d3af5127d20da1e54224e76192484cf352ce00c167995507ad03c523235f.bin | 3cb9d3af5127d20da1e54224e76192484cf352ce00c167995507ad03c523235f | US20210106952A1:Comparative Example 13 | shutdown_temperature | Shutdown temperature (° C.) | 140 | ° C. | 140 | C | https://patents.google.com/patent/US20210106952A1/en | null | TABLE 4 | null | 26 | 5 | patent_html_table | separator-v32 | null | null | PE/PP | reviewed_sample_link | [{"locator": "p-0208", "text": "A polyolefin microporous membrane was obtained under the same conditions as in Comparative Example 12 except that the surface layer (B layer) contained 92 parts by weight of polyethylene having has the melting point of 135° C., viscosity-average molecular weight of 250,000, and molecular... | null | trilayer; PE/PP-blend outer layers | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0036 | FIG. 1(A) is a schematic diagram illustrating a measurement apparatus of a shutdown temperature, FIG. 1(B) is a schematic view explaining a microporous membrane fixed on a nickel foil in measurement of a shutdown temperature, and FIG. 1(C) is a schematic view explaining masking of a nickel foil in measurement of a shut... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0 C."} | null | accepted | Publication US20210106952A1; Comparative Example 13; printed unit: ° C.. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p-0208 | 66100808 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 445144d3c4ae18d4a041a53c11de9c28ef09538a19f56fe735c6f48badb17f67; current SHA256 identifies sanitized bytes. | 0053ad9dbe58fde936c91a28575b892c0a5bad9e15b9ec95dfc268c49cdf8188 | 3 | not_reported_in_linked_identity | |||||
b33b938ab1f07ede038fc8cbd8a5950e69aa5e84b16715a70f2e7e29d4a25b07 | b2399ad9851ef082e208dd246ffafe0791cbafb3b5a839e243c1597fe5d0c765 | patents | data/raw/ebb73d5f17b49377879cc4f855a8458da11e09c9b623649751252ddd440b00cb.bin | ebb73d5f17b49377879cc4f855a8458da11e09c9b623649751252ddd440b00cb | US20090170005A1:Comparative Example 3 | thickness | Average Thickness (μm) | 20.2 | μm | 20.2 | um | https://patents.google.com/patent/US20090170005A1/en | null | TABLE 1 | null | 65 | 4 | patent_html_table | separator-v32 | null | null | PE | explicit_composition_table | [{"locator": "TABLE-US-00001", "text": "TABLE 1 No. Example 1 Example 2 Example 3 Example 4 Resin Composition PE Composition UHMWPE Mw (1) 2.5 × 10 6 2.5 × 10 6 2.0 × 10 6 2.5 × 10 6 % by mass 30 20 20 20 HDPE Mw (1) 2.8 × 10 5 2.8 × 10 5 2.8 × 10 5 3.0 × 10 5 % by mass 70 80 80 80 LMPE Mw (1) — — — — % by mass — — — —... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0165 | (1) Average Thickness (μm) The thickness of the microporous polyethylene membrane was measured at a 5-mm interval over a width of 30 cm by a contact thickness meter, and the measured thickness was averaged. | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Publication US20090170005A1; Comparative Example 3; printed unit: μm. Example identity and experimental protocol retained; no processing temperature inferred. | 38005816 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 394234338c2143cf6c4ae5ce5baef870eb584e97443328ff4fe31d33e0366928; current SHA256 identifies sanitized bytes. | 0054173fcebcbbe646375ec8b8cf6aabcc6f89250a77046ed36f75a4fbb522bb | 2 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
14e74491f8496365c8898b588d3d9d08be76a5ce3ecc7ee323606410bf6851ce | ddd906c259ca0adbeb904016e0e277734b964ced193569736eb0f8791a9610d1 | patents | data/raw/f5780c0a3c96bd5ac638575dd1292a76dc29e0b42e1d25668eb8eae6f467a5f2.bin | f5780c0a3c96bd5ac638575dd1292a76dc29e0b42e1d25668eb8eae6f467a5f2 | US20070264483A1:Example 5 | porosity | Porosity (%) | 35.7 | % | 35.7 | % | https://patents.google.com/patent/US20070264483A1/en | null | TABLE 1 | null | 75 | 2 | patent_html_table | separator-v32 | null | null | PE/PP | explicit_composition_table | [{"locator": "TABLE 1", "text": "Composition rows 48, 51, 57"}] | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0126 | (3) Porosity (%) Measured by a weight method. | null | measured | null | null | null | null | null | accepted | Publication US20070264483A1; Example 5; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Composition rows 48, 51, 57 | 38685493 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 d0566823fdb941115eb4d924f29a753382c1e4577bc64ea13cb181350f4f2dcc; current SHA256 identifies sanitized bytes. | 005423309e4e09d99e6eb58bdc179f7e3dd2316687f0c3d1f7510a0aefdbd828 | 1 | not_reported_in_linked_identity | |||||
ecba3f1db996f55c84c22c359dd93802dba065d594286598ac5ceb2a4889dbbf | 29cabffb9ca93599452a8b179f5ba540fee9a0d8fa3dff1fd0315fff4e0da092 | patents | data/raw/70a2f68b8c64dc53e8564279929c46c02198f3ec833411a676d59ae1b349d7a0.bin | 70a2f68b8c64dc53e8564279929c46c02198f3ec833411a676d59ae1b349d7a0 | US11242440B2:Example 12 | meltdown_temperature | Meltdown temperature (° C.) | 182 | ° C. | 182 | C | https://patents.google.com/patent/US11242440B2/en | null | TABLE 2 | null | 67 | 4 | patent_html_table | separator-v32 | null | null | PE | explicit_recipe | [{"locator": "p-0151", "text": "Polyethylene was synthesized using the polyethylene synthesis catalyst listed in any one of Tables 1 to 4 (represented as “synthesis catalyst” in the tables) and an ethylene monomer. As shown in Tables 1 to 4, in each Example, two types of polyethylenes wherein one polyethylene type was ... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0033 | (10) Meltdown Temperature (° C.) FIG. 1 (A) shows a schematic diagram illustrating a meltdown temperature measurement apparatus. 1 denotes a microporous membrane, 2 A and 2 B denote nickel foils with a thickness of 10 μm, and 3 A and 3 B denote glass plates. An electric resistance measurement device 4 (LCR meter “AG-43... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0 C."} | null | accepted | Publication US11242440B2; Example 12; printed unit: ° C.. Example identity and experimental protocol retained; no processing temperature inferred. | 63674906 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 28f3184b80b10819376843b18950734bae6c8d3770f7535bfd5543a02504f063; current SHA256 identifies sanitized bytes. | 0059c6cc14a4ebc5e2fbfe457a1774d5b36e315ecb69218e8e5639e55f736592 | 1 | not_reported_in_linked_identity | |||||
c79739e68ae2fe9d8e7ab632cd76625830760f075955e2f861a74ab0fbbf0f52 | 4d5898f1b88c7e55b198170f62cd64f19e23798fca6074e0c06da76222b07f33 | manual | data/runs/2026-10-23_balanced_verified/raw/c045fd45729a9f777ef0bef0d9f0a492b166f1075c7921c19780595858261004.csv | c045fd45729a9f777ef0bef0d9f0a492b166f1075c7921c19780595858261004 | US20220411600A1:Example 3 | thermal_shrinkage | thermal_shrinkage | 7.5 | % | 7.5 | % | https://patents.google.com/patent/US20220411600A1/en | null | TABLE 4 | null | 25 | 5 | manual_structured_import | separator-v32 | null | null | PE/PP | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "TABLE 4", "source_file": "data/runs/2026-10-23_balanced_verified/raw/c045fd45729a9f777ef0bef0d9f0a492b166f1075c7921c19780595858261004.csv", "source_sha256": "c045fd45729a9f777ef0bef0d9f0a492b166f1075c7921c197805958... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | null | separator | not_reported | null | null | null | reported | 120 | exposure | 60 | null | TD | Reviewed source-explicit physical membrane property tables and experimental methods | The PO microporous membrane was cut out to 100 mm in the MD direction and 100 mm in the TD direction, and allowed to stand for 1 hour in an oven at a prescribed temperature (120° C. or 150° C.). During this time, the sample was sandwiched between two sheets of paper so as to avoid direct contact of the sample with warm... | length | measured | null | null | null | null | null | accepted | Primary SHA256 4b8b14942d1d30e42e91bb60c6836baa7c0223a16b4bae5bb3880df82dee9f96; raw table row 17, column 5; label TD heat shrinkage factor at 120° C.; printed value/unit 7.5 %; recipe evidence TABLE-US-00003. Air permeability units denote time for 100 cm3, not per-thickness normalized values. | null | null | Reviewed primary patent membrane results only; excludes resin inputs, TMA stress, thickness-normalized forces and battery results; preserve primary evidence hashes. | 005b5b24221d289bb1d126d29cb8f57f9df299d01997f75355fcc6ddd7153be6 | 1 | not_reported_in_linked_identity | |||||
bf84f69888f14dbb4681ca7dfd85faee8ec91f6c3ab37eb14a09b9cad0545075 | b9c9c4560f506105d85814d37d19b254da9472d3ee8ee7c65c34d42017c7e3ff | patents | data/runs/2026-10-26_balanced/raw/e5796a7a0ae6f989f1a9cce633de859118a0a93fc12520268ef0e056a4004cc3.bin | e5796a7a0ae6f989f1a9cce633de859118a0a93fc12520268ef0e056a4004cc3 | US20240079723A1:Example 5 | porosity | Porosity | 45.8 | % | 45.8 | % | https://patents.google.com/patent/US20240079723A1/en | null | TABLE 3 | null | 11 | 7 | patent_html_table | separator-v32 | null | null | null | sample_label_not_found | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | 23 | measurement | null | null | unspecified | Patent experimental protocol h-0036 | [Porosity (%) (Before Compression)] A 3 cm×3 cm square, 1 cm×1 cm square, 5 cm×5 cm square, or 10 cm×10 cm square sample was cut from the polyolefin microporous membrane, the volume (cm 3 ) and mass (g) thereof were determined, and these values and the density (g/cm 3 ) were used in the following formula: Porosity (%)=... | null | measured | null | null | null | null | null | accepted | Publication US20240079723A1; Example 5; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed conditions: {"basis": "Source explicitly declares a physical-test temperature default; property-specific method checked for overrides. US20240079723 porosity rows a... | 88651776 | null | License/reuse permission not established; local research evidence only | 005c9f732661df9d0b9a719d6738f3f176407fb4a8c9da4fa40c091196b3d6f1 | 1 | not_reported_in_linked_identity | |||||
23aee2e892b06d042d91eb8d2ab8c73cc6e430bcea0785093e201c8f7cb4a846 | 1e8663847c9962402ab71942f628ddf6e8a43191d0a983a8d0abdf82faa8c755 | patents | data/runs/2026-10-26_balanced/raw/628d56ef80773282f099224189b0dc919b03fa90ba76e4860b143296893a3394.bin | 628d56ef80773282f099224189b0dc919b03fa90ba76e4860b143296893a3394 | EP2551293A1:Example 18 | thermal_shrinkage | Complex membrane Heat shrinkage ratio [%] | 16 | % | 16 | % | https://patents.google.com/patent/EP2551293A1/en | null | table_4 | null | 15 | 4 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "num:p0106", "text": "As a polyethylene powder, GUR2126 (weight-averaged molecular weight: 4,150,000, number average molecular weight: 800,000, melting point: 141°C; manufactured by Ticona corporation) which is ultra-high molecular weight polyethylene and GURX143 (weight-averaged molecular weight: 560,000,... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 105 | exposure | 60 | null | unspecified | null | (13) Heat shrinkage ratio The heat shrinkage ratios of the polyolefin microporous membrane and the separator for non-aqueous secondary battery were measured by heating the sample at 105°C for 1 hour. The measurement direction is in the machine direction. | null | measured | null | null | null | null | null | accepted | Publication EP2551293A1; Example 18; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 44673280 | null | License/reuse permission not established; local research evidence only | 005efe7c09bba97e37f6bd96762dd14fca18f59b4f17d979709337d583fab2b3 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
7379a396dbd87660b2f1f1329d37e929288160223532fcda279ea956b0e34c69 | df0ff1aa37aa2ddb26510d26c7dd5c6ae26a344f318c34328e1781adce8af047 | patents | data/raw/fa2ec9764a0312f292d2596873e0efa5c2ec366a0fd665968b8de60b74e5de5f.bin | fa2ec9764a0312f292d2596873e0efa5c2ec366a0fd665968b8de60b74e5de5f | US11183734B2:Example 3 | puncture_force | test Pin puncture strength (mN) 5394 3727 4070 4913 | 5394 | mN | 5.394 | N | https://patents.google.com/patent/US11183734B2/en | null | TABLE 3 | null | 11 | 9 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p-0152", "text": "To 100 parts by mass of a composition consisting of 30% by mass of ultra high molecular weight polyethylene having a mass average molecular weight of 2.7×10 6 and 70% by mass of high density polyethylene having a mass average molecular weight of 2.6×10 5 , 0.375 parts by mass of tetrakis... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0122 | On the other hand, when a microporous membrane after the heat compression under a pressure of 4.0 MPa at 80° C. for 10 minutes is used, the relative impedance ratio C at room temperature and a high temperature (80° C.) (the ratio of the relative impedance A (%) measured at a high temperature (80° C.) to the relative im... | null | measured | null | null | null | {"offset": 0, "scale": 0.001} | null | accepted | Publication US11183734B2; Example 3; printed unit: mN. Example identity and experimental protocol retained; no processing temperature inferred. | 61301827 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 d95de61a643cd9efaaa045b3f1a37c092d49cd830cb00e311087f39af9b44272; current SHA256 identifies sanitized bytes. | 006485cd16dfd4d5ce86cc320ae72e81929854f97adc80ba82e8660ec16742f4 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
d20988b52a522838fb2994af19c81cab7cb030ebf0fac16b7890b7ea204b2c78 | c555e58813abf95dd64fa18cc2b0c9b0349ac167a358a767cb1782cef5c1e41c | patents | data/runs/2026-10-23_balanced/raw/3040883f6876a37ffad977713cbd26204c52a718432b427a81d47b70ab3ec4d7.bin | 3040883f6876a37ffad977713cbd26204c52a718432b427a81d47b70ab3ec4d7 | EP4375059A1:Comparative Example 1 | tensile_strength | Physic al proper ties Tensile strength (MPa) Tensile strength (MPa) Tensile strength (MPa) TD TD | 121 | MPa | 121 | MPa | https://patents.google.com/patent/EP4375059A1/en | null | table_3 | null | 29 | 7 | patent_html_table | separator-v32 | null | null | PE/PP | reviewed_sample_link | [{"locator": "p0116", "text": "A raw material obtained by dry-blending 0.2 mass% of tetrakis(methylene-3-(3,5-di-tert-butyl-4-hydroxyphenyl)-propionate)methane as an antioxidant with 100 mass% of a polyolefin composition composed of 70 mass% of ultrahigh molecular weight polyethylene having a weight average molecular w... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | TD | Patent experimental protocol h0043 | (7) [Tensile rupture strength (MPa), tensile rupture elongation (%), toughness (MPa•%)] The tensile rupture strength (MPa) and the tensile rupture elongation (%) corresponding to MD and TD were measured in accordance with ASTM D 882 under the following conditions using an tensile tester Instron 5543 manufactured by Ins... | null | measured | null | null | null | null | null | accepted | Publication EP4375059A1; Comparative Example 1; printed unit: MPa. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p0116 | p0117 | p0118 | p0120 | p0124 | p0125 | p0127 | p0130 | 84979946 | null | License/reuse permission not established; local research evidence only | 006a9c860696d8fabc106d7012e6d1c274b1d229c49698e2ff638d5f9f24d8e1 | 1 | not_reported_in_linked_identity | UHMWPE/isotactic PP | ||||
a44d5b54798898ae2e906ff4dbf7cf9baeb8df8ce4ac9e955a7cae8e7ace96bf | c555e58813abf95dd64fa18cc2b0c9b0349ac167a358a767cb1782cef5c1e41c | patents | data/runs/2026-10-23_balanced/raw/3040883f6876a37ffad977713cbd26204c52a718432b427a81d47b70ab3ec4d7.bin | 3040883f6876a37ffad977713cbd26204c52a718432b427a81d47b70ab3ec4d7 | EP4375059A1:Comparative Example 4 | elongation | Physic al proper ties Tensile elongation (%) Tensile elongation (%) Tensile elongation (%) MD+TD MD+TD | 186 | % | 186 | % | https://patents.google.com/patent/EP4375059A1/en | null | table_3 | null | 33 | 10 | patent_html_table | separator-v32 | null | null | PE/PP | reviewed_sample_link | [{"locator": "p0116", "text": "A raw material obtained by dry-blending 0.2 mass% of tetrakis(methylene-3-(3,5-di-tert-butyl-4-hydroxyphenyl)-propionate)methane as an antioxidant with 100 mass% of a polyolefin composition composed of 70 mass% of ultrahigh molecular weight polyethylene having a weight average molecular w... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h0043 | (7) [Tensile rupture strength (MPa), tensile rupture elongation (%), toughness (MPa•%)] The tensile rupture strength (MPa) and the tensile rupture elongation (%) corresponding to MD and TD were measured in accordance with ASTM D 882 under the following conditions using an tensile tester Instron 5543 manufactured by Ins... | null | measured | null | null | null | null | null | accepted | Publication EP4375059A1; Comparative Example 4; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p0116 | p0117 | p0118 | p0120 | p0124 | p0125 | p0127 | p0130 | p0131 | p0132 | p0133 | 84979946 | null | License/reuse permission not established; local research evidence only | 006ff94c5d93ab515c3c618ce70c12e336ac3d6ae43a7d7856e73337521b0ae1 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE/isotactic PP | ||||
03093a813c1a9bf09f6d83686d6f8e5cdcb5d3ec8942085cc5209bcae534283a | 942e67905af2386071ee31d0e54d3218fcadfae24266ca7aeefa5164ee37bda9 | patents | data/runs/2026-10-23_balanced_temperature/raw/cc99a44978559381884361600fc53dab0773b65713a80771d26113464a130d62.bin | cc99a44978559381884361600fc53dab0773b65713a80771d26113464a130d62 | US20250038360A1:Example 9 | porosity | configuration Porosity % | 53 | % | 53 | % | https://patents.google.com/patent/US20250038360A1/en | null | TABLE 10 | null | 25 | 5 | patent_html_table | separator-v32 | null | null | PE | explicit_recipe | [{"locator": "p-0559", "text": "The same operation as in Example 4 was carried out, except that, as shown in Tables 9 to 15, the resin composition conditions for forming the microporous layer (CL) capable of forming a crosslinked structure, the conditions of polyethylene (PE) for forming the polyethylene microporous la... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0081 | <Porosity (%)> A 10 cm×10 cm square sample was cut out from a separator for an electricity storage device, and the volume (cm 3 ) and weight (g) thereof were determined and used together with the density (g/cm 3 ) by the following formula to obtain a porosity. The density value used for the mixed composition was the va... | null | measured | null | null | null | null | null | accepted | Publication US20250038360A1; Example 9; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 78084758 | null | License/reuse permission not established; local research evidence only | 0078c9321d51bdb8e2c589b3ff77dcdb8eb67eb9400c1cc885350060967df892 | 1 | PE layer component: semicrystalline; state during test unverified | explicit_identity_or_reviewed_sample_evidence | [{"crystallinity_pct": 70.0, "locator": "TABLE 10", "method": "source-reported PE layer", "publication": "US20250038360A1", "sample": "Example 9", "scope": "PE layer component", "source_sha256": "cc99a44978559381884361600fc53dab0773b65713a80771d26113464a130d62", "evidence_source_file": "data/runs/2026-10-23_balanced_te... | [{"crystallinity_pct": 70.0, "locator": "TABLE 10", "method": "source-reported PE layer", "publication": "US20250038360A1", "sample": "Example 9", "scope": "PE layer component", "source_sha256": "cc99a44978559381884361600fc53dab0773b65713a80771d26113464a130d62", "evidence_source_file": "data/runs/2026-10-23_balanced_te... | ||
68e11ca8a0fb6c79426495cbaffbe3d3433154d1306453315da7bc7b8eecfcc5 | 903aca71e375e64cc23a533e14b7f7d988ef48d030696fe23af39827cdc52d6a | manual | data/runs/2026-10-23_balanced_verified/raw/2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d704fa1.csv | 2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d704fa1 | PMC9076374:LAGP/PP | ionic_conductivity | ionic_conductivity | 0.91 | mS/cm | 0.091 | S/m | https://www.ebi.ac.uk/europepmc/webservices/rest/PMC9076374/fullTextXML | null | tab2 | null | 53 | 4 | manual_structured_import | separator-v32 | null | Celgard 2500 | PP | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "tab2", "source_file": "data/runs/2026-10-23_balanced_verified/raw/2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d704fa1.csv", "source_sha256": "2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d7... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | LAGP | null | null | separator | electrolyte_wet | null | null | null | reported | null | unknown | null | null | unspecified | Reviewed primary XML table/result; reported scalar only | SS blocking electrodes; electrolyte-saturated separator impedance; room temperature unnumbered. Not whole-cell charge-transfer resistance. | null | measured | null | null | null | {"offset": 0, "scale": 0.1} | null | accepted | Primary XML SHA256 b167073daf6e125006ec181a2100a00592244148142076a6258a4e148fd9ba0d; XML row 5, column 4; printed cell 0.91; exact evidence: LAGP/PP 27 1.6 0.91 | null | null | Reviewed primary XML table extracts; preserve exact source coordinates and hashes; original source reuse terms apply. | 007c1ceb64e121e689cc12d0a33c7ba1b75738de0374c1d8cad1bf23e196a683 | 1 | not_reported_in_linked_identity | |||||
b28d17ab8d89f0eab140c84d2734fa2881c1d9ef41948e8699865a4ac06c318a | c147a82844d25b480414ccf0b9c35ad30856f8f2e5f7877b9cf6d47aeec4dddf | patents | data/runs/2026-10-23_balanced/raw/24ef2d13021dd7dbaf3c75cc10fe024e708429276674fe72ae72c99f519fc70e.bin | 24ef2d13021dd7dbaf3c75cc10fe024e708429276674fe72ae72c99f519fc70e | US11616273B2:Example 6 | thickness | Heat-resistant layer thickness (μm) | 4 | μm | 4 | um | https://patents.google.com/patent/US11616273B2/en | null | TABLE 2 | null | 8 | 4 | patent_html_table | separator-v32 | null | null | null | not_linked_to_recipe | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0096 | The thickness was measured according to GB/T6672-2001. Thickness Analyzer (VL-50-B, available from Mitutoyo, Japen) was used to measure the thickness of the separators. The measurement was conducted by a probe with diameter of 3 mm with a measuring force of 0.01 N. | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Publication US11616273B2; Example 6; printed unit: μm. Example identity and experimental protocol retained; no processing temperature inferred. | 74550557 | null | License/reuse permission not established; local research evidence only | 008b8083e6b2a3ee995c152b5b2cc684d459297c34bf7efb1054ffcd18da0d06 | 1 | not_reported_in_linked_identity | |||||
81cabc857a4388c2ecfb8754fa6487f3e9095e631575d145fc3fa199344eaf1e | 3ca677c0f442efb15a1209e35cf1c61aa9c33e2a0915d1b160baf53ff222af3e | patents | data/raw/d0343cdc947553af700e941b1b000c1ef32923da78ee9520d0c0948d2c24bf47.bin | d0343cdc947553af700e941b1b000c1ef32923da78ee9520d0c0948d2c24bf47 | US20090134538A1:Example 6 | thickness | Average Thickness (μm) | 0.08 | μm | 0.08 | um | https://patents.google.com/patent/US20090134538A1/en | null | TABLE 2 | null | 64 | 3 | patent_html_table | separator-v32 | null | null | PE/PP | inherited_recipe | [{"locator": "p-0123", "text": "100 parts by mass of polypropylene (PP) having a mass-average molecular weight (Mw) of 5.7×10 5 were dry-blended with 0.2 parts by mass of tetrakis[methylene-3-(3,5-ditertiary-butyl-4-hydroxyphenyl)-propionate] methane with as an antioxidant. The melting point of PP was 165° C."}, {"loca... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0137 | (1) Average Thickness (μm) The thickness of the multi-layer, microporous membrane was measured at a 5-mm longitudinal interval over a width of 30 cm by a contact thickness meter, and the measured thickness was averaged. | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Publication US20090134538A1; Example 6; printed unit: μm. Example identity and experimental protocol retained; no processing temperature inferred. | 37962566 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 b4e9cec5353afc839c29d236d8886811cddbe10d4e285ee76c450c2c8550b99f; current SHA256 identifies sanitized bytes. | 008bc650c2126cdfeb8393af01414ef834e27398973179eda9208491f7f0aab9 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
cb77839ed3be756dc4dd858a8a80d742b9ce4e2994ad66c1b21e531d6fd7df53 | fe6206ba1f1864ace01ac1b791b80df8f223e12f381d17c5f2d1a1842c367dce | patents | data/runs/2026-10-23_balanced_temperature/raw/cdcfe71fb5af9f21a65319f2c02486d640f930ba8a36ae939dd08c689e4f28a9.bin | cdcfe71fb5af9f21a65319f2c02486d640f930ba8a36ae939dd08c689e4f28a9 | EP2866278B1:Comparative Example 3 | thermal_shrinkage | Properties of polyolefin microporous membrane Shrinkage ratio (TD) % | 10 | % | 10 | % | https://patents.google.com/patent/EP2866278B1/en | null | table_1 | null | 30 | 9 | patent_html_table | separator-v32 | null | null | PE | explicit_composition_table | [{"locator": "css:html:nth-of-type(1) > body:nth-of-type(1) > search-app:nth-of-type(1) > article:nth-of-type(1) > section:nth-of-type(5) > div:nth-of-type(1) > ul:nth-of-type(1) > tables:nth-of-type(1) > patent-tables:nth-of-type(1) > table:nth-of-type(1)", "text": "Examples 1-7, Comparative Examples 1-2 Example 8 Exa... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 130 | exposure | null | 5 | TD | Patent experimental protocol h0037 | (3) Shrinkage Rate at 130°C The transverse shrinkage rate at 130°C (measured by thermomechanical analysis under a load of 2 gf at a temperature rise rate of 5°C/min) of the polyolefin microporous membrane used in the present invention is 20% or less. If it is more than 20%, when the modifying porous layer is laminated ... | null | measured | null | null | null | null | null | accepted | Publication EP2866278B1; Comparative Example 3; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 50941631 | null | License/reuse permission not established; local research evidence only | 008ca4e2095e4d29f87b31215faa8626674bd18d2d87fd6eedec9d889041211a | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
541155a7851101248b9166e6ac0f77b0f654365b07f525185094a49314384797 | a17b5e5736c5669610ed7f148388712e675ca3365331c05027f5e8fcb1d92c94 | manual | data/runs/2026-10-23_balanced_verified/raw/b543503a34f6f1366742383ad9f9e92eb916ff1ab5ac0a0fe7fd585a59d33c58.csv | b543503a34f6f1366742383ad9f9e92eb916ff1ab5ac0a0fe7fd585a59d33c58 | US20130021719A1:Ex. 1 | density | density | 0.34 | g/cm3 | 340 | kg/m3 | https://patents.google.com/patent/US20130021719A1/en | null | summary experimental table | null | 3 | 3 | manual_structured_import | separator-v32 | null | null | PP | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "summary experimental table", "source_file": "data/runs/2026-10-23_balanced_verified/raw/b543503a34f6f1366742383ad9f9e92eb916ff1ab5ac0a0fe7fd585a59d33c58.csv", "source_sha256": "b543503a34f6f1366742383ad9f9e92eb916f... | Material supplied by source adapter or reviewed import; see source coordinates and notes | beta-nucleated PP film for double-layer capacitors | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Reviewed primary table and explicit measurement protocol | Primary DLC separator film study; PP homopolymer / propylene-ethylene block copolymer, not a PP/PE laminate. Processing roll temperatures excluded. | null | measured | null | null | null | {"offset": 0, "scale": 1000} | null | accepted | Primary SHA256 23bb50b5bd2e8b42a4b59ee502b7df79af4b179ced0039e8ea2470cedda2218b; exact expanded table row 8, column 3; raw scalar 0.34 g/cm3. Source scope retained in measurement context. | null | null | Reviewed primary exact table cells; retain primary hashes and scope; no inferred numeric ambient temperature and no OCR-corrupted resistance units accepted. | 008fe3e5e8b07aec775e06c0e3f7d7972cfb96464f94eee9c03e6ec2213d7f34 | 3 | not_reported_in_linked_identity | |||||
7ddf5d7809d73e4673269af1fc031f7fedd58475cf62c0127e19fbc424d96641 | 7a49c4d4d597c44bb6603f8703b456853022d931c3ffa4ee8445b276ad968936 | patents | data/raw/c04d88bed714c6731dc13de65bd771b73f14c41179171a73910456ff5e5c273e.bin | c04d88bed714c6731dc13de65bd771b73f14c41179171a73910456ff5e5c273e | US20130189587A1:Comparative Example 1 | thermal_shrinkage | 105° C. TD Heat Shrinkage (%) | 1.0 | % | 1 | % | https://patents.google.com/patent/US20130189587A1/en | null | TABLE 1 | null | 29 | 4 | patent_html_table | separator-v32 | null | null | PE | explicit_recipe | [{"locator": "p-0077", "text": "As shown in Table 1, Examples 1 and 2 demonstrate that a microporous membrane having a thickness 19.0 micrometer or less can be produced, the membrane having a porosity 43.0% or more, a puncture strength 1.7×10 2 mN/micrometer or more, and a normalized air permeability 10.0 seconds/100 c... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 105 | exposure | null | null | TD | Patent experimental protocol h-0030 | Maximum TMA Heat Shrinkage Maximum TMA Heat Shrinkage in a planar direction of the membrane (e.g., MD and/or TD) is measured by the following procedure. For Maximum TD Heat Shrinkage, a rectangular sample of about 3.0 mm×about 50.0 mm is cut out of the microporous membrane such that the long axis of the sample is align... | length | measured | null | null | null | null | null | accepted | Publication US20130189587A1; Comparative Example 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 44563199 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 0015b04f6a4e2c4912d831eb0b2ba016c2a050d57ddd25fbdc0e7629a72cf8fa; current SHA256 identifies sanitized bytes. | 009d492db689bf522fa9c4076acbaaf7939c6cb243fc7cc1fcbb32679590a12c | 1 | not_reported_in_linked_identity | |||||
0f624a42758ad1313a68a341363642e2fc07efb0a55fabfe86b89111ae93083d | 2077a4cf73e70a05b2093a3aeb83f83551938a58deb7be22c6b73b4b46e1d1e2 | patents | data/raw/041c55935fe5a639bba4e7a041ec3b11a43a47e431363ebe4bfd2e3bbf224ecc.bin | 041c55935fe5a639bba4e7a041ec3b11a43a47e431363ebe4bfd2e3bbf224ecc | US10507436B2:Example 2 | porosity | Porosity % (%) | 40.5 | % | 40.5 | % | https://patents.google.com/patent/US10507436B2/en | null | TABLE 1 | null | 14 | 4 | patent_html_table | separator-v32 | null | null | null | sample_label_not_found | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0042 | (2) Porosity (%) The porosity was determined using the following equation, in which the weight w 1 of the microporous membrane and the weight w 2 of an equivalent polymer having no pores (polymer having the same width, length, and composition) were compared. Porosity (%)=( w 2 −w 1 )/ w 2 ×100 (3) Air Permeation Resist... | null | measured | null | null | null | null | null | accepted | Publication US10507436B2; Example 2; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 56150800 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 91a057645ef5e000f026766b517aa1a950d04247c6828fc214529db59a6a2c7b; current SHA256 identifies sanitized bytes. | 009f2145826e28747d916a50b4e3cb30a585df5aec70003c758409469901417f | 1 | not_reported_in_linked_identity | |||||
49adb3ec7345e609d5acbc140da2a53b3adfdc4ebc6b5a99ce5cf7e953bdb244 | 6804f755a7ab02b766f1556b14fec765b1afc58dbb70d69e23133193f43220a7 | manual | data/runs/2026-10-23_balanced_verified/raw/67477b2e5873991140efeaf8a69cb69125780a739565f7fdd747e903d8d8ad81.csv | 67477b2e5873991140efeaf8a69cb69125780a739565f7fdd747e903d8d8ad81 | US20250066568A1:Comparative Example 6 | tortuosity | tortuosity | 6.7 | 1 | 6.7 | 1 | https://patents.google.com/patent/US20250066568A1/en | null | p-0196 | null | 380 | 4 | manual_structured_import | separator-v32 | null | null | PE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "p-0196", "source_file": "data/runs/2026-10-23_balanced_verified/raw/67477b2e5873991140efeaf8a69cb69125780a739565f7fdd747e903d8d8ad81.csv", "source_sha256": "67477b2e5873991140efeaf8a69cb69125780a739565f7fdd747e903d... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | null | separator_component | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Primary patent Parameter Tests of Polyethylene-Based Film; source result tables 2A–4B | null | null | calculated | null | null | null | null | null | accepted | Primary source SHA256 a3e09c2a3f6ae90f04b66edebcdb76f822a79400161d1ee6de3130bdd1ae2633; XML/HTML locator p-0196, expanded row 13; exact cells: Tortuosity | 6.5 | 6.8 | 6.7; material from Table 1 p-0187, Example 14 explicitly PP; no numeric mechanical test temperature reported. | null | null | Reviewed primary experimental base-film tables; preserve source SHA and exact coordinates; source reuse terms apply. | 00a24a7c0afdb1257c64732954490136071dc968e9461f8486607100a0736427 | 2 | not_reported_in_linked_identity | |||||
1c7041a8d8b799949ee3be382776b26b308e64f2a11819e9eac500ffe3e0eb84 | c402693dfdd1c6dea31a16a3426d486db2f348a1b75616ee147a123bf1172e13 | patents | data/runs/2026-10-23_balanced/raw/b5d47e7ea06035e17e7ee5e3de7050c5450479fe54f3faec539967c2ccdc579d.bin | b5d47e7ea06035e17e7ee5e3de7050c5450479fe54f3faec539967c2ccdc579d | US20140072878A1:Example 1 | thickness | Sheet thickness (μm) | 28 | μm | 28 | um | https://patents.google.com/patent/US20140072878A1/en | null | TABLE 1 | null | 10 | 2 | patent_html_table | separator-v32 | null | null | null | coating_material_only | [{"locator": "p-0093", "text": "NBKP was dispersed in ion-exchanged water so as to have a concentration of 3% by weight. The dispersion was subjected to a refining treatment by cycling under the conditions so that the number average fiber length ranged from 1.0 to 1.2 mm, by means of a double disk refiner. The dispersi... | Named polymer is in coating preparation; base substrate material has not been established | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0015 | (5) Measurement of Thickness The thickness of the separator sample with a size of 50 mm×50 mm was measured at any 5 points by means of a thickness indicator TM600 (manufactured by Kumagai Riki Kogyo Co., Ltd.). An average value obtained from the aforementioned 5 values of thickness measured was used as a membrane thick... | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Publication US20140072878A1; Example 1; printed unit: μm. Example identity and experimental protocol retained; no processing temperature inferred. | 48081933 | null | License/reuse permission not established; local research evidence only | 00b822f26bdcde01b28a5387e38c877e55316aef2d7c7d6af9e7042c2a923ffa | 2 | not_reported_in_linked_identity | |||||
df8a464be1a8163ad75f2d540186ea70497cfdca443f6e632a74594f3411761e | 1377fc49cc188be3568757283f01757ac545081b8454b408f060658736b9f1d6 | patents | data/runs/2026-10-19_expansion/raw/78fc83b885911a313b35805edc6a46500e6c3f29a8aeb5ca9a46ba9c8109181a.bin | 78fc83b885911a313b35805edc6a46500e6c3f29a8aeb5ca9a46ba9c8109181a | EP3181621A1:Example 3 | thermal_shrinkage | Shrinkage Shrinkage at 105°C in the TD (%) | 9.1 | % | 9.1 | % | https://patents.google.com/patent/EP3181621A1/en | null | table_2 | null | 5 | 6 | patent_html_table | separator-v32 | null | null | PE | reviewed_sample_link | [{"locator": "p0072", "text": "A polyethylene composition consisting of 30 wt.% of a PE 1 (ultrahigh molecular weight polyethylene, weight average molecular weight (Mw): 2.89 × 10 6 , molecular weight distribution (Mw/Mn): 5.28) as an ultrahigh molecular weight polyethylene and 70 wt.% of a PE2 (high-density polyolefin... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 105 | exposure | 480 | null | TD | Patent experimental protocol h0018 | 6. Thermal shrinkage The shrinkage in the MD when the microporous membrane was held for 8 hours at 105°C was measured three times, and the average was used as the thermal shrinkage in the MD. In addition, similar measurements were taken in the TD to determine the thermal shrinkage in the TD. | null | measured | null | null | null | null | null | accepted | Publication EP3181621A1; Example 3; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p0072 | p0074 | 55304161 | null | License/reuse permission not established; local research evidence only | 00bdcf5ffc27bc3ecba12d895ced28cc80982f1aa4541da349e90c1066016d11 | 1 | not_reported_in_linked_identity | UHMWPE | ||||
a7ab257c02a53c782122997b644c768da4ce870155437632a168cb8d909a7cad | 1377fc49cc188be3568757283f01757ac545081b8454b408f060658736b9f1d6 | patents | data/runs/2026-10-19_expansion/raw/78fc83b885911a313b35805edc6a46500e6c3f29a8aeb5ca9a46ba9c8109181a.bin | 78fc83b885911a313b35805edc6a46500e6c3f29a8aeb5ca9a46ba9c8109181a | EP3181621A1:Example 4 | thermal_shrinkage | Shrinkage Shrinkage at 105°C in the MD (%) | 5.0 | % | 5 | % | https://patents.google.com/patent/EP3181621A1/en | null | table_2 | null | 6 | 5 | patent_html_table | separator-v32 | null | null | PE | reviewed_sample_link | [{"locator": "p0072", "text": "A polyethylene composition consisting of 30 wt.% of a PE 1 (ultrahigh molecular weight polyethylene, weight average molecular weight (Mw): 2.89 × 10 6 , molecular weight distribution (Mw/Mn): 5.28) as an ultrahigh molecular weight polyethylene and 70 wt.% of a PE2 (high-density polyolefin... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 105 | exposure | 480 | null | MD | Patent experimental protocol h0018 | 6. Thermal shrinkage The shrinkage in the MD when the microporous membrane was held for 8 hours at 105°C was measured three times, and the average was used as the thermal shrinkage in the MD. In addition, similar measurements were taken in the TD to determine the thermal shrinkage in the TD. | null | measured | null | null | null | null | null | accepted | Publication EP3181621A1; Example 4; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p0072 | p0075 | 55304161 | null | License/reuse permission not established; local research evidence only | 00cffe3ca2c47e2bf93b56b4dfe31723e6a4d22f4c87aa6e2eda471eabe2db9e | 1 | not_reported_in_linked_identity | UHMWPE | ||||
e1007c3e22e9b030b2be8e7b6934fa2184258f2eb848352cc0952b30ff58151c | 45ee7887a4fb7e651d5f0c4e75a79ac51b890a8d7075e9f8180ff17fa5d2982e | patents | data/runs/2026-10-19_expansion/raw/b940ec54fb1af9ae605e13dfd241035aa8e3aa2d1f4d89c73d62531f7f8ace54.bin | b940ec54fb1af9ae605e13dfd241035aa8e3aa2d1f4d89c73d62531f7f8ace54 | US20060154140A1:Comparative Example 1 | puncture_force | puncture strength (N) | 6.37 | N | 6.37 | N | https://patents.google.com/patent/US20060154140A1/en | null | TABLE 2 | null | 43 | 4 | patent_html_table | separator-v32 | null | null | null | not_linked_to_recipe | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0089 | (5) Puncture strength: a nonwoven was cut out into a size of 30 mm (length)×100 mm (width); on the sample thus prepared, an aluminum press plate (length: 46 mm, width: 86 mm, thickness: 7 mm) having a 11 mm-diameter hole in its middle was placed; a peak load (N) was measured when a needle was caused to pierce the middl... | null | measured | null | null | null | null | null | accepted | Publication US20060154140A1; Comparative Example 1; printed unit: N. Example identity and experimental protocol retained; no processing temperature inferred. | 32171040 | null | License/reuse permission not established; local research evidence only | 00d0cabc146cf928dcdda00ac2fbc3772e110783761c5e87e2ae4032cdd3ec99 | 1 | not_reported_in_linked_identity | |||||
0db2ee05d3c14664aaa5b326a7c7e03a67442d6591ef885d8c41d6e975614b0e | 1116e9e34676f48e4b02dfd5ae14e5dac45de6f2f279931ec15c63f9bd0b6b9a | fsri | data/runs/2026-10-30_thermal/raw/b3800fc0ce8e6f7c4891893df97e7448c360fe43c7dd745214647004c3f0f903.csv | b3800fc0ce8e6f7c4891893df97e7448c360fe43c7dd745214647004c3f0f903 | LDPE_STA_N2_30KData_210908_R2 | sta_mass_percent | Mass(subtr.2)/% | 99.31132 | % | 99.31132 | % | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/LDPE/STA/N2/30K_min/LDPE_STA_N2_30KData_210908_R2.csv | null | null | null | LDPE_STA_N2_30KData_210908_R2.csv:CSV row 759 | Mass(subtr.2)/% | fsri_sta_native_csv | separator-v32 | null | null | LDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "LDPE_STA_N2_30KData_210908_R2.csv:CSV row 759", "source_file": "data/runs/2026-10-30_thermal/raw/b3800fc0ce8e6f7c4891893df97e7448c360fe43c7dd745214647004c3f0f903.csv", "source_sha256": "b3800fc0ce8e6f7c4891893df97e... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 124.965 | measurement | null | 30 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R2 | fsri:STA:LDPE_STA_N2_30KData_210908_R2 | null | null | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 f... | null | fsri:STA:LDPE_STA_N2_30KData_210908_R2:row:759:sta_mass_percent | License/reuse permission not established; local research evidence only | 00d284e692193845fa801c984606198134ae9c6536250fa77ce48f3d12da92bc | 1 | LDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "LDPE", "labels": ["LDPE"]}, {"field": "sample_id", "text": "LDPE_STA_N2_30KData_210908_R2", "labels": ["LDPE"]}] | LDPE | ||
be3269a5cb416e6585867ad66727fdfcb6543536fd4f52383f4b100087e9f539 | 903aca71e375e64cc23a533e14b7f7d988ef48d030696fe23af39827cdc52d6a | manual | data/runs/2026-10-23_balanced_verified/raw/2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d704fa1.csv | 2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d704fa1 | PMC9076374:PP | contact_angle | contact_angle | 58 | deg | 58 | deg | https://www.ebi.ac.uk/europepmc/webservices/rest/PMC9076374/fullTextXML | null | tab1 | null | 23 | 3 | manual_structured_import | separator-v32 | null | Celgard 2500 | PP | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "tab1", "source_file": "data/runs/2026-10-23_balanced_verified/raw/2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d704fa1.csv", "source_sha256": "2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d7... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Reviewed primary XML table/result; reported scalar only | null | null | measured | null | null | null | null | null | accepted | Primary XML SHA256 b167073daf6e125006ec181a2100a00592244148142076a6258a4e148fd9ba0d; XML row 2, column 3; printed cell 58; exact evidence: PP 25 58 102 45 5 | null | null | Reviewed primary XML table extracts; preserve exact source coordinates and hashes; original source reuse terms apply. | 00df7c01942643d3c85c2938519b580092075c24b94ecdc99d59ada93e3f2507 | 1 | not_reported_in_linked_identity | |||||
3125bce5df40bacbc0192621867a62c918684683cebefb74283dd6d91e7fdba8 | dceb396a8981b259ec248549d088560a330b7821e63fac67520cd2432273e037 | manual | data/runs/2026-10-26_pdf_verified/raw/73ee191d4c972ae18890eafd105f7bb31d7aedd57d830b1da066b9e70cfc328b.csv | 73ee191d4c972ae18890eafd105f7bb31d7aedd57d830b1da066b9e70cfc328b | US20200343511A1:TABLE 2:Example 16 | thermal_shrinkage | thermal_shrinkage | 17 | % | 17 | % | https://patents.google.com/patent/US20200343511A1/en | null | TABLE 2 | null | 178 | 8 | manual_structured_import | separator-v32 | null | null | PP/PE/PP | reviewed_pdf_sample_link | [{"source_file": "data/runs/2026-10-26_pdf/raw/b2e88270585c36140db61b50aaef41bd35d4b321ca185f4c4a2725868cfc68ed.pdf", "source_sha256": "b2e88270585c36140db61b50aaef41bd35d4b321ca185f4c4a2725868cfc68ed", "page": 15, "locator": "PDF page 15, TABLE 2, sample Example 16; rendered material and measurement rows inspected", "... | Material row/experimental material section explicitly matched to this sample in the original PDF | PP/PE/PP coated trilayer | PVDF / BaSO4, both sides | null | null | separator | not_reported | null | null | null | reported | 150 | exposure | null | null | unspecified | Reviewed primary PDF TABLE 2; source method retained in notes when specified | Primary PDF page 15, TABLE 2; printed separator property. Numeric test temperature unreported unless a dedicated condition is supplied. | area | measured | null | null | null | null | null | accepted | Primary PDF SHA256 b2e88270585c36140db61b50aaef41bd35d4b321ca185f4c4a2725868cfc68ed; PDF page 15; primary table row 16, column 8; original printed cell 17 %. Material attribution checked in rendered original PDF, not inferred from title. | null | null | Reviewed primary-source PDF cells; original reuse restrictions apply; raw PDFs retained locally | 00e0f45422884ea8aa22ac0742cda47ba1d64f4b6e5d602fb1f457472ee58ece | 1 | not_reported_in_linked_identity | |||||
9cb25ca9958ee699ce9c4a05689c1bcc1c9559bd1175d803a4380fd3c8842a47 | 31f62894e14a619fd9d0b0b6afa74ff677eb64bcb2f12583375e2f9e8ac07429 | patents | data/runs/2026-10-26_balanced/raw/9d7265b573347c1e7a667d935c529244d673ce5dab9054288fa881da7b5458b4.bin | 9d7265b573347c1e7a667d935c529244d673ce5dab9054288fa881da7b5458b4 | US20040053122A1:Example 5 | air_permeability_time | Air permeability (sec/100 ml) | 140 | sec/100 ml | 140 | s | https://patents.google.com/patent/US20040053122A1/en | null | TABLE 2 | null | 15 | 3 | patent_html_table | separator-v32 | null | null | null | not_linked_to_recipe | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol P-0116 | (2) Air Permeability of Separator [0116] Air permeability, weight per 1 m [0117] 2 of the porous layer (PFVd), an impregnation ratio and a retention ratio of the electrolytic solution, and ionic conductivity of the resulting separator were evaluated. The air permeability was measured by using Gurley Densometer, Model B... | null | measured | null | null | null | {"canonical_unit": "s", "unit_alias": "sec/100 ml"} | null | accepted | Publication US20040053122A1; Example 5; printed unit: sec/100 ml. Example identity and experimental protocol retained; no processing temperature inferred. | 31949589 | null | License/reuse permission not established; local research evidence only | 00e99efe37d07029344091e6f23fdeaef50d3f61895ee24328501bf13d0aa5fc | 1 | not_reported_in_linked_identity | |||||
5c3af6519683e71db0008a4f7f286944a1b4dff44f9db61f526c441511cca4e2 | 84ba5a9ae3bf8af20265becaad2dcdc5a239e0b3668b7abb22f699f118c620a8 | patents | data/raw/91e776380da1e1e247a3ab3a3c5edfd97beb24b00c9c3b01f789f3a1e5f4f894.bin | 91e776380da1e1e247a3ab3a3c5edfd97beb24b00c9c3b01f789f3a1e5f4f894 | US20110033743A1:Comparative example 2 | meltdown_temperature | Meltdown temperature | 155 | ° C. | 155 | C | https://patents.google.com/patent/US20110033743A1/en | null | TABLE 2 | null | 31 | 4 | patent_html_table | separator-v32 | null | null | null | generic_polyolefin_only | [{"locator": "p-0120", "text": "The same the polyolefin microporous film as in the comparative example 1 is used, and the solution for forming the coating layer is prepared by dissolving non-aromatic polyvinyldene fluoride-hexafluoropropylene (P(VdF-co-HFP)) having a melting temperature of 160° C. in NMP solvent. In th... | Sample recipe names polyolefin but does not establish a specific PE/PP composition | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0106 | (9) Shutdown Temperature and Meltdown Temperature Shutdown temperature and meltdown temperature of the microporous polyolefin composite film is measured in a simple cell which can measure impedance. In the simple cell, the microporous polyolefin composite film is interposed between two graphite electrodes, and electrol... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0 C."} | null | accepted | Publication US20110033743A1; Comparative example 2; printed unit: ° C.. Example identity and experimental protocol retained; no processing temperature inferred. | 41162398 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 acadff71a630d2759c966f99377b72df705f5b650aac458d052ec3f16b9539f3; current SHA256 identifies sanitized bytes. | 00eb8b28259c45609a23c52c48bd19811d89549695f3e161673d54b65b9ad6e5 | 1 | not_reported_in_linked_identity | |||||
02185d24a058838a315f8b2014d7db528f56f636baebbbba7ceb0d0311c4eb0d | 8aa91e212b6563df40db3d07ec80c41c88a37ab63182cfdf9783477819d6fe86 | patents | data/raw/f6d13bf8b637df94f9e412f899fe6ef1b2974beb7081153061e695aa10c12efb.bin | f6d13bf8b637df94f9e412f899fe6ef1b2974beb7081153061e695aa10c12efb | US20090269656A1:Example 7 | elongation | Tensile Rupture Elongation (%) MD/TD | 177 | % | 177 | % | https://patents.google.com/patent/US20090269656A1/en | null | TABLE 1 | null | 126 | 2 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p-0113", "text": "Dry-blended were 100 parts by mass of a polyethylene composition comprising 18% by mass of ultra-high-molecular-weight polyethylene (UHMWPE) having a mass-average molecular weight (Mw) of 2.0×10 6 and Mw/Mn of 8, and 82% by mass of high-density polyethylene (HDPE) having Mw of 3.0×10 5 a... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | MD | Patent experimental protocol p-0139 | (5) Tensile Rupture Strength and Tensile Rupture Elongation They were measured using a 10-mm-wide rectangular test piece according to ASTM D882. | null | measured | null | null | null | null | null | accepted | Publication US20090269656A1; Example 7; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Printed MD/TD cell: 177/244. | 37865034 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 7fbbe7bfab2d1b50edbc3eced477f751bdc7716cb81e9021d0ceef1084bbcd7c; current SHA256 identifies sanitized bytes. | 00eef8a3ec9e381d105f074285884aca0de330a4727e4ee18d5e3f3827e6953d | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
00a6e558f15ace52214e6c0b4051f1517057daba255a510c4aae8cd32fea8188 | 6e7b6da08dc925414688fa26db21b2a82e8744fc1adaed5b7e2d21a7f9cf5a44 | patents | data/runs/2026-10-23_balanced/raw/7aa8f22f50865b65daf9e5292f2567e41a623cd0a9110f0696a4921eca0467f6.bin | 7aa8f22f50865b65daf9e5292f2567e41a623cd0a9110f0696a4921eca0467f6 | EP2261276B1:Example 36 | thickness | Physical properties of polyolefin microporous film Film thickness Film thickness µm | 7 | µm | 7 | um | https://patents.google.com/patent/EP2261276B1/en | null | table_7 | null | 24 | 8 | patent_html_table | separator-v32 | null | null | PE/PP | explicit_composition_table | [{"locator": "css:html:nth-of-type(1) > body:nth-of-type(1) > search-app:nth-of-type(1) > article:nth-of-type(1) > section:nth-of-type(5) > div:nth-of-type(1) > ul:nth-of-type(1) > li:nth-of-type(168) > div:nth-of-type(1) > tables:nth-of-type(4) > patent-tables:nth-of-type(1) > table:nth-of-type(1)", "text": "Item Unit... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 23 | measurement | null | null | unspecified | null | (2) Film thickness (µm) A film thickness was measured at room temperature of 23°C using a micro thickness meter KBM (trademark) made by Toyo Seiki Seisaku-sho, Ltd. | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u00b5m"} | null | accepted | Publication EP2261276B1; Example 36; printed unit: µm. Example identity and experimental protocol retained; no processing temperature inferred. | 41135394 | null | License/reuse permission not established; local research evidence only | 00f58ec028803975f0439d1b69f63fb7e3ccec5e227e0534831d3cf41db25a8e | 10 | not_reported_in_linked_identity | |||||
0de67ee32c607044db15798a637531741e526faf7321618110a6e511babc7f76 | 3d060534de6feb226df5a584371d1991c086cc08c545b361896c58f8abd028fa | patents | data/raw/35b5b4e89d5425e0d246b399713cdc58b073884172bd8f03b632c2173037851a.bin | 35b5b4e89d5425e0d246b399713cdc58b073884172bd8f03b632c2173037851a | US11139533B2:Comparative Example 1 | thermal_shrinkage | MD Heating 6.2 4.3 5.5 6.9 6.1 4.1 7.2 3.4 6.8 shrinkage ratio (%) | 5.9 | % | 5.9 | % | https://patents.google.com/patent/US11139533B2/en | null | TABLE 2 | null | 28 | 14 | patent_html_table | separator-v32 | null | null | PE/PP | inherited_recipe | [{"locator": "p-0249", "text": "Using a T-die having a discharge width of 1000 mm and a discharge lip opening of 2 mm, a polypropylene resin having a weight-average molecular weight of 590,000, a molecular weight distribution of 11.0, a pentad fraction of 92%, and a melting point of 161° C. was melted and extruded at a... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 105 | exposure | 60 | null | MD | Patent experimental protocol p-0237 | A gauge with a gauge distance of 180 mm was marked on the center portion at one point in each of the width direction (TD) and the length direction (MD) of each of the test pieces, and the gauge dimension was measured with a steel scale. The specimen with the marked gauge length was wrapped by paper and was subjected to... | length | measured | null | null | null | null | null | accepted | Publication US11139533B2; Comparative Example 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 59627725 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 ec62a02d96dc61315630aeffb8ec65f95f4ace64b3b477f8baf517fef4349120; current SHA256 identifies sanitized bytes. | 00fafc36cf3029488e3567d6a6284bc6ada3f84c909ca3780e4c61a9b894bb1d | 1 | not_reported_in_linked_identity | HDPE | ||||
04f2e2cf5d2d7bf23360d8672dc19e7e149cdd4b11ac4cb103054626239e10b9 | d9a11f955b058bba53350f78f19559c48316cf5e19ee4d0db16205569c4ca12b | fsri | data/runs/2026-10-30_thermal/raw/9ef68fcb1551c422ffae6d466b2d08207dc6ed172e4941e69f37a68518fdedc3.csv | 9ef68fcb1551c422ffae6d466b2d08207dc6ed172e4941e69f37a68518fdedc3 | HDPE_STA_N2_10KData_2199_R1 | mass_specific_heat_flow | DSC(subtr.2)/(mW/mg) | 0.62836 | mW/mg | 628.36 | W/kg | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/HDPE/STA/N2/10K_min/HDPE_STA_N2_10KData_2199_R1.csv | null | null | null | HDPE_STA_N2_10KData_2199_R1.csv:CSV row 2206 | DSC(subtr.2)/(mW/mg) | fsri_sta_native_csv | separator-v32 | null | null | HDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "HDPE_STA_N2_10KData_2199_R1.csv:CSV row 2206", "source_file": "data/runs/2026-10-30_thermal/raw/9ef68fcb1551c422ffae6d466b2d08207dc6ed172e4941e69f37a68518fdedc3.csv", "source_sha256": "9ef68fcb1551c422ffae6d466b2d0... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 270.008 | measurement | null | 10 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R1 | fsri:STA:HDPE_STA_N2_10KData_2199_R1 | null | {"offset": 0.0, "scale": 1000.0} | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 b... | null | fsri:STA:HDPE_STA_N2_10KData_2199_R1:row:2206:mass_specific_heat_flow | License/reuse permission not established; local research evidence only | 00fcbb79647568f7080c51fddf429f968a70e773471bb28ba70f133c8671ceaf | 1 | HDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "HDPE", "labels": ["HDPE"]}, {"field": "sample_id", "text": "HDPE_STA_N2_10KData_2199_R1", "labels": ["HDPE"]}] | HDPE | ||
1f6ca060d2ba0e7dbeefe3a46b62f51ebf90d922f55e2fff3ecbaffbd6d554bd | cdb93fdd628c5a6d3de45f945e4cfa7588c090d795c5e84e17d67cad2d6502ec | patents | data/raw/72866a495be6bba11761b81edd5a3e216164cb6086075a6d51e287641cb6458a.bin | 72866a495be6bba11761b81edd5a3e216164cb6086075a6d51e287641cb6458a | US20090098341A1:Example 2 | melting_temperature | Melting Point (° C.) | 135 | ° C. | 135 | C | https://patents.google.com/patent/US20090098341A1/en | null | TABLE 1 | null | 13 | 3 | patent_html_table | separator-v32 | null | null | PE | explicit_composition_table | [{"locator": "TABLE-US-00001", "text": "TABLE 1 No. Example 1 Example 2 Example 3 Example 4 PE Composition UHMWPE Molecular Weight (Mw) 2.0 × 10 6 2.0 × 10 6 2.0 × 10 6 2.0 × 10 6 Mw/Mn 8 8 8 8 Content (wt. %) 18 18 18 18 HDPE Molecular Weight (Mw) 3.0 × 10 5 3.0 × 10 5 3.0 × 10 5 3.0 × 10 5 Mw/Mn 8.6 8.6 13.5 8.6 Cont... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0028 | Though not particularly restricted, the melt-blending method preferably comprises even melt-blending in an extruder. This method is suitable for preparing a high-concentration PO solution. The melt-blending temperature of the PO is preferably in a range of the melting point of PO +10° C. to +100° C. Specifically, the ... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0 C."} | null | accepted | Publication US20090098341A1; Example 2; printed unit: ° C.. Example identity and experimental protocol retained; no processing temperature inferred. | 37073341 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 0c3c59f7959c7ce0301bac417684d48f5bba25b4ee45364a3c0fec274bc20c55; current SHA256 identifies sanitized bytes. | 0100834ad9b703f8db69f8c088b3a16a15c5a73e0b118bbdb472389d20cbaf07 | 8 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
2250622da522f16d6ca467c0d8722ce5234d088dc690d5732c5d9e6a9551afaa | b9d025a9d17c28b956ce970b1de67ad8f0c521dedc57e888669bcdae6492ef0e | patents | data/raw/087245f0f484f1930251d3f351f56e4879d8fcb932ab82a1833994d96c201e98.bin | 087245f0f484f1930251d3f351f56e4879d8fcb932ab82a1833994d96c201e98 | US8778525B2:Com. Ex. 4 | elongation | Tensile Rupture Elongation (%) MD/TD | 130 | % | 130 | % | https://patents.google.com/patent/US8778525B2/en | null | TABLE 1 | null | 259 | 3 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "num:p-0157", "text": "Dry-blended were 100 parts by mass of a polyethylene (PE) composition comprising 25% by mass of ultra-high-molecular-weight polyethylene (UHMWPE) having a mass-average molecular weight (Mw) of 2.0×10 6 , and 75% by mass of high-density polyethylene (HDPE) having Mw of 3.5×10 5 , with... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | MD | Patent experimental protocol p-0194 | (6) Tensile Rupture Strength and Tensile Rupture Elongation They were measured using a 10-mm-wide rectangular test piece according to ASTM D882. | null | measured | null | null | null | null | null | accepted | Publication US8778525B2; Com. Ex. 4; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Printed MD/TD cell: 130/160. | 37771661 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 bc72da7f119fe7244ad7e32b7148c8b5dccd980c3bed9846ef8b311a93fd4938; current SHA256 identifies sanitized bytes. | 01010830c9588fd985721bb43059c4620607309fa9a9490a49044f1d66bafb73 | 2 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
cf16f1d507a7064d67feb86060f58838d3eff286b746a89368d97e6b1e37521b | ab5d07a8f8e47cd1462c004ec7c39811f1a5e2a70e7a0b51a47e6d3c6d5aaa7c | patents | data/raw/0a8a43a71685068c8d272d5eaed6d6ad158cf59515a876ad50e4e739e44790da.bin | 0a8a43a71685068c8d272d5eaed6d6ad158cf59515a876ad50e4e739e44790da | US20120115008A1:Comparative Example 7 | basis_weight | Basis weight | 7.1 | g/m 2 | 7.1 | g/m2 | https://patents.google.com/patent/US20120115008A1/en | null | TABLE 2 | null | 33 | 4 | patent_html_table | separator-v32 | null | null | PE | reviewed_sample_link | [{"locator": "p-0223", "text": "As a polyethylene powder, GUR2126 (weight-averaged molecular weight: 4,150,000, melting point: 141° C.) and GURX143 (weight-averaged molecular weight: 560,000, melting point: 135° C.) manufactured by Ticona were used. A polyethylene solution was produced by making the mixing ratio of GUR... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0182 | (3) Basis Weight The basis weights (mass per 1 m 2 ) of the polyolefin microporous membrane and the separator for a non-aqueous secondary battery were obtained by measuring the mass of a sample cut out in 10 cm×10 cm and dividing the measured mass by the area. | null | measured | null | null | null | {"canonical_unit": "g/m2", "unit_alias": "g/m 2"} | null | accepted | Publication US20120115008A1; Comparative Example 7; printed unit: g/m 2. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p-0223 | p-0229 | p-0238 | 44673209 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 2f67082b26eb472cc609c03b0999afa775ae991bb61b38d1c4eef1ee2b37c899; current SHA256 identifies sanitized bytes. | 01038c07c77defa6ed679bd058f6d9ba548d916d5f4fd1a395d37c0e29d73f32 | 1 | not_reported_in_linked_identity | |||||
3cb46a8ee92328fce49f45002f03256ffabe9fa646ae6377ede04683eb6add64 | 921a4164de6826e7b71815568a1c1e34cf73d13558019c1cb8094c169fd12148 | patents | data/raw/16110b0be4c99b724a4933df170764839a6988affc75f2feb72bf05e316d40b1.bin | 16110b0be4c99b724a4933df170764839a6988affc75f2feb72bf05e316d40b1 | US20090274955A1:Example 3 | thermal_shrinkage | Heat Shrinkage Ratio (%) MD/TD | 3 | % | 3 | % | https://patents.google.com/patent/US20090274955A1/en | null | table_1 | null | 52 | 4 | patent_html_table | separator-v32 | null | null | PE/PP | inherited_recipe | [{"locator": "p-0151", "text": "Dry-blended were 100 parts by mass of a polyethylene composition comprising 20% by mass of ultra-high-molecular-weight polyethylene (UHMWPE) having a mass-average molecular weight (Mw) of 2.0×10 6 , and 80% by mass of high-density polyethylene (HDPE) having Mw of 3.5×10 5 , and 0.2 parts... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 105 | exposure | 480 | null | MD | Patent experimental protocol p-0191 | (6) Heat Shrinkage Ratio (%) The shrinkage ratio of the multi-layer, microporous membrane after exposed to 105° C. for 8 hours was measured three times in both longitudinal direction (MD) and transverse direction (TD) and the obtained 3 values were averaged. | null | measured | null | null | null | null | null | accepted | Publication US20090274955A1; Example 3; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Printed MD/TD cell: 3/4. | 37668759 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 7f0c3770bfa0d8aa70587cdeaf6388cca6e5d1fa48546a3a9cba39e68fbc158c; current SHA256 identifies sanitized bytes. | 01044e546a71f15c95b640041ff201fbc3581b99a97543a17ca2c43f77ce43cc | 2 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
161f81612a20a695e4ef9e42a5c015e50cdc4051dbf6d09edead70471158e572 | 9a1ab0fd11426a2013d185dc0e8d6f3cfa8fa6709112c0a4c3648317c6fe3cb6 | manual | data/raw/6dd8d700c137e19e8dc3b5079f8574e3ed033dff0fccef680da9b44ee78ff280.csv | 6dd8d700c137e19e8dc3b5079f8574e3ed033dff0fccef680da9b44ee78ff280 | ma12193125:bare_PE | elongation | elongation | 77.4 | % | 77.4 | % | https://www.ebi.ac.uk/europepmc/webservices/rest/PMC6804153/fullTextXML | null | materials-12-03125-t002 | null | 7 | null | manual_structured_import | separator-v32 | null | null | PE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "materials-12-03125-t002", "source_file": "data/raw/6dd8d700c137e19e8dc3b5079f8574e3ed033dff0fccef680da9b44ee78ff280.csv", "source_sha256": "6dd8d700c137e19e8dc3b5079f8574e3ed033dff0fccef680da9b44ee78ff280"}] | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Primary paper methods section; rectangular 8 cm x 2 cm; tensile/puncture at 25 mm/min | null | null | measured | null | null | null | null | null | accepted | Reviewed primary source https://www.ebi.ac.uk/europepmc/webservices/rest/PMC6804153/fullTextXML; original file data/runs/2026-10-19_literature/raw/15a8bc8ba95334b0c7058529c6091d1ba242fcdfb5107008f225b29d1bebd467.bin; SHA256 15a8bc8ba95334b0c7058529c6091d1ba242fcdfb5107008f225b29d1bebd467; evidence: Tensile elongation a... | null | null | Source-specific reuse terms apply; original primary XML/HTML and hashes retained in notes and evidence sidecar. | 010832fb8c9adecefba281421f365a43b958ee59a6f1cd933268900dfd39456d | 1 | not_reported_in_linked_identity | |||||
9c8951fd03e4ed9b1484699b378651f06e67a3e100d53efa8ffc8bbf26a14c13 | 674bf2b86c2010112d7e940abdced2682335c1092612a3229bc73bb2482d54b2 | patents | data/runs/2026-10-26_balanced/raw/bab8da665b0fe63aecac96acef0134ba6ec510a76203fff48b44742319fc5b4e.bin | bab8da665b0fe63aecac96acef0134ba6ec510a76203fff48b44742319fc5b4e | US10826108B2:Ex. 1 | tensile_strength | Tensile Strength in TD (kgf/cm2) | 951 | kgf/cm2 | 93.261242 | MPa | https://patents.google.com/patent/US10826108B2/en | null | TABLE 1 | null | 14 | 3 | patent_html_table | separator-v32 | null | null | PE | explicit_recipe | [{"locator": "p-0086", "text": "A 13 um Celgard® EK1321 PE microporous membrane was coated with a 4 μm coating layer consisting of Polybenzimidazole (available as a 26% dope in DMAc from PBI Performance Products in Rock Hill, S.C.) and Degussa fumed Alumina 20 nm diameter particles. The coating solution is prepared by ... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | TD | Patent experimental protocol p-0101 | Tensile Properties Machine Direction (MD) and Transverse Direction (TD) tensile strength is measured using Instron Model 4201 according to ASTM-882 procedure. | null | measured | null | null | null | {"offset": 0, "scale": 0.0980665} | null | accepted | Publication US10826108B2; Ex. 1; printed unit: kgf/cm2. Example identity and experimental protocol retained; no processing temperature inferred. | 45559769 | null | License/reuse permission not established; local research evidence only | 011710bd93fdc8beeb4a81de81fc9e7981906f5cb5094a4a651b354370f9ffab | 1 | not_reported_in_linked_identity | |||||
f09e58ffee07e14a99e889dbbed7c2616ef3cc22ef3436f9ef05774ff4746c00 | f1e57db8b563c7b5662149c55274c6f6e5e0c8a911c2785da7445f6f6a4ee0c5 | patents | data/raw/c333dce6046ebf9183a04cfa8c7aff7c8c6c0e3c7505e1f9042d14594a5485b5.bin | c333dce6046ebf9183a04cfa8c7aff7c8c6c0e3c7505e1f9042d14594a5485b5 | US8748028B2:Comparative Ex 1 | porosity | Porosity % | 56.7 | % | 56.7 | % | https://patents.google.com/patent/US8748028B2/en | null | TABLE 2 | null | 9 | 2 | patent_html_table | separator-v32 | null | null | PE/PP | reviewed_sample_link | [{"locator": "num:p-0168", "text": "A first polyolefin composition comprising (a) 50% first polyethylene resin having a weight average molecular weight of 3.0×10 5 and a molecular weight distribution of 8.6, (b) 37.5% first polypropylene resin having a weight average molecular weight of 1.1×10 6 , a heat of fusion of 1... | null | trilayer; mixed PE/PP layers | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0204 | (3) Porosity (%) Measured by a weight method using the formula: Porosity %=100×(w2−w1/w2, wherein “w1” is the actual weight of film and “w2” is the assumed weight of 100% polyethylene. | null | measured | null | null | null | null | null | accepted | Publication US8748028B2; Comparative Ex 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: num:p-0168 | num:p-0180 | num:p-0183 | num:p-0190 | 40588396 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 26df8961d1a3e7e892ed34bec7552de81beda739fe964c9445d38a5eb11b708d; current SHA256 identifies sanitized bytes. | 011c800651496427dd13d2e5a7be9fe05b663443b65a691aea684023e321f7fa | 1 | not_reported_in_linked_identity | |||||
559ee9305cf910514e075b323f8f0007f0f2ba873b24bf1a56358b2865f2663e | a06dbef9dcc39089c7e6fdda8691b3445ec5f2200be6cee257b3a2d46068f4dc | patents | data/raw/39c9749677f68f7e8c98dfa1e9778d1a05c732b56cfed0e50e86acaba1dfed27.bin | 39c9749677f68f7e8c98dfa1e9778d1a05c732b56cfed0e50e86acaba1dfed27 | US10256447B2:Ex. 1 | thickness | Thickness, μm | 16 | μm | 16 | um | https://patents.google.com/patent/US10256447B2/en | null | TABLE 2 | null | 5 | 2 | patent_html_table | separator-v32 | null | null | null | sample_label_not_found | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0062 | Thickness is measured using the Emveco Microgage 210-A precision micrometer thickness tester according to test procedure ASTM D374. Thickness values are reported in units of micrometers, μm. | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Publication US10256447B2; Ex. 1; printed unit: μm. Example identity and experimental protocol retained; no processing temperature inferred. | 57441855 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 f5f28fed5fc00f223ec1e88ab1519eafc159fcb3173741edc47e6abcc3ce9746; current SHA256 identifies sanitized bytes. | 012a4deab9e0c891f85d54baf04a239a528eee7199424fb3e0f9015fa667ffcc | 2 | not_reported_in_linked_identity | |||||
4eb1a5e0b5d2d73929e7a9b0cadde8e8eb8295133167dd1bfea7cf8b6ab1bb0b | 76453948daa2633eead708782f5f4b9cdf0961674706a797c7f849f7d79101d9 | fsri | data/runs/2026-10-30_thermal/raw/27c883726cb903590038ac77266eb517c9a00c2232bdab86a3540d7a333770ac.csv | 27c883726cb903590038ac77266eb517c9a00c2232bdab86a3540d7a333770ac | LDPE_STA_N2_3KData_210908_R2 | heat_flow | DSC(subtr.2)/mW | -0.49737 | mW | -0.000497 | W | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/LDPE/STA/N2/3K_min/LDPE_STA_N2_3KData_210908_R2.csv | null | null | null | LDPE_STA_N2_3KData_210908_R2.csv:CSV row 506 | DSC(subtr.2)/mW | fsri_sta_native_csv | separator-v32 | null | null | LDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "LDPE_STA_N2_3KData_210908_R2.csv:CSV row 506", "source_file": "data/runs/2026-10-30_thermal/raw/27c883726cb903590038ac77266eb517c9a00c2232bdab86a3540d7a333770ac.csv", "source_sha256": "27c883726cb903590038ac77266eb... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 100.006 | measurement | null | 3 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R2 | fsri:STA:LDPE_STA_N2_3KData_210908_R2 | null | {"offset": 0.0, "scale": 0.001} | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 7... | null | fsri:STA:LDPE_STA_N2_3KData_210908_R2:row:506:heat_flow | License/reuse permission not established; local research evidence only | 01391b9cd875f936a31f627d954d7782435d7cfeedd7eac2a37c28d8c8a36f8f | 1 | LDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "LDPE", "labels": ["LDPE"]}, {"field": "sample_id", "text": "LDPE_STA_N2_3KData_210908_R2", "labels": ["LDPE"]}] | LDPE | ||
c510e58a0106ab2d88d0883be1ce9469b515272527f5c478bc62e1ebff93c9cb | a737d88d53f5ae36519b7396fa048c05ba162df917ea3d32fe8bfcf28466d761 | patents | data/runs/2026-10-23_balanced/raw/bd4dff14bfedec857c5569f248e85c2fbd417883fc5bc6ea9af6fc51fa14a371.bin | bd4dff14bfedec857c5569f248e85c2fbd417883fc5bc6ea9af6fc51fa14a371 | EP3912813A1:Comparative example 7 | meltdown_temperature | property meltdown temperature (°C) | 179.0 | °C | 179 | C | https://patents.google.com/patent/EP3912813A1/en | null | table_2 | null | 26 | 10 | patent_html_table | separator-v32 | null | null | null | changed_recipe_needs_link | [{"locator": "p0100", "text": "Except that the ultrahigh molecular weight polypropylene used in Example 1 for preparing a polyolefin resin solution for the first layer was replaced with an ultrahigh molecular weight polypropylene (isotactic, mesopentad fraction 86.0%) with a Mw of 2.0 × 10 6 , the same procedure as in ... | Inherited recipe changes material composition; exact resulting recipe not yet linked | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h0035 | (7) Shutdown temperature and meltdown temperature While heating a microporous film at a heating rate of 5°C/min, the air permeation resistance was measured with an Oken type air permeation resistance gauge (EGO-1T, manufactured by Asahi Seiko Co., Ltd.), and the temperature at which the air permeation resistance reache... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0C"} | null | accepted | Publication EP3912813A1; Comparative example 7; printed unit: °C. Example identity and experimental protocol retained; no processing temperature inferred. | 71613059 | null | License/reuse permission not established; local research evidence only | 0142993c7859f90e1c18b581ea251f1e672c713373933513177829fad8c61aa8 | 1 | not_reported_in_linked_identity | |||||
99f60db1ea83b2de35cceaa116a50ca23cfc2c3806afa661e519fa247e407be3 | ea5b766a349dd6d04e8198d3701065ebbc34c2c9a7ff09b53ab90fd51e60256a | celgard | data/raw/f2a939ae19fe83219f13e467ea5ffd2fdf87326222e4b4a22c74183ae94e67bb.pdf | f2a939ae19fe83219f13e467ea5ffd2fdf87326222e4b4a22c74183ae94e67bb | celgard_S2010 | thickness | Thickness | 20 | μm | 20 | um | https://www.celgard.com/storage/components/s2010_com_data_2026-01.pdf | 1 | 1 | null | 2 | 3 | pymupdf.find_tables | separator-v32 | Celgard | S2010 | PP/PE/PP | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "1", "source_file": "data/raw/f2a939ae19fe83219f13e467ea5ffd2fdf87326222e4b4a22c74183ae94e67bb.pdf", "source_sha256": "f2a939ae19fe83219f13e467ea5ffd2fdf87326222e4b4a22c74183ae94e67bb"}] | Material supplied by source adapter or reviewed import; see source coordinates and notes | trilayer | null | null | polyolefin separator | separator | not_reported | null | null | null | typical | null | unknown | null | null | unspecified | null | Thickness | null | unknown | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Manufacturer table; source unit as printed: μm. Typical specifications do not establish an experimental measurement temperature. | null | null | License/reuse permission not established; local research evidence only | 0143a212de8ea605318f103ce45ca6dbb1fce82c0db980f666bf5370526a6a4b | 1 | not_reported_in_linked_identity | |||||
8dca6e89d8bfdef441b8ae730356e92be8b5cab6ca5d8aac77f82f098ed8df9a | 71b9c0b3c4b8081f55169ffe3e37a7da471ff3bed25274b8ad6c847c2ac9609b | patents | data/raw/8884b228944135feb9236c289b75c0563a820d0d6aa0a50f0fe9adfa9a2a7684.bin | 8884b228944135feb9236c289b75c0563a820d0d6aa0a50f0fe9adfa9a2a7684 | US20160164060A1:Ex. 17 | thickness | Coating thickness, μm | 5.6 | μm | 5.6 | um | https://patents.google.com/patent/US20160164060A1/en | null | TABLE 5 | null | 21 | 5 | patent_html_table | separator-v32 | null | null | PE | reviewed_sample_link | [{"locator": "p-0112", "text": "Example 17 is a PE microporous base membrane having an uncoated thickness of 9 μm, which is single-side coated with an aqueous coating formulation having a 20:80 weight percent ratio of polyvinylidene fluoride (PVDF) polymer to aluminum oxide (Al 2 O 3 ) ceramic particles. The coating fo... | null | coated microporous membrane | PVDF/alumina | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0030 | Thickness Test Thickness is measured using the Emveco Microgage 210-A precision micrometer thickness tester according to test procedure ASTM D374. Thickness values are reported in units of micrometers, μm. | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Publication US20160164060A1; Ex. 17; printed unit: μm. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p-0112 | 56092503 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 d666a350f788857eecf69455daf6783e897a64f69070c214cdc87aea8b65a540; current SHA256 identifies sanitized bytes. | 0148a256b487f0011f6b54323f15468ca0425bb9597d77afebf15e09532bca5b | 1 | not_reported_in_linked_identity | |||||
c991e1c209be1ccd6206ca97d341168160a71345d04205e4c1abb86efc46261b | 1999403bbf6741d93292e8b3b11df7e0589fa58190f86feaa34bc22a35141e96 | fsri | data/runs/2026-10-26_source_probe_fsri/raw/61ae2124210c7b5665a770d119c62b588d6e32d49a3ea200562d6dd7f6340b1e.tst | 61ae2124210c7b5665a770d119c62b588d6e32d49a3ea200562d6dd7f6340b1e | PUF_Mattress_Pad_HFM_Wet_HeatCapacity_220602_R1.tst | volumetric_heat_capacity | heatcapacity | 41406.0 | J/(m3 K) | 41,406 | J/(m3 K) | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/PUF_Mattress_Pad/HFM/PUF_Mattress_Pad_HFM_Wet_HeatCapacity_220602_R1.tst | null | Results Table -- SI Units | null | PUF_Mattress_Pad_HFM_Wet_HeatCapacity_220602_R1.tst:row 3 | null | fsri_hfm_si | separator-v32 | null | null | PUF_Mattress_Pad | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "Results Table -- SI Units", "source_file": "data/runs/2026-10-26_source_probe_fsri/raw/61ae2124210c7b5665a770d119c62b588d6e32d49a3ea200562d6dd7f6340b1e.tst", "source_sha256": "61ae2124210c7b5665a770d119c62b588d6e32... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 30.01 | measurement | null | null | through-plane | TA Instruments FOX HFM; SI results | FSRI Wet; ambient/unconditioned Wet is not electrolyte soaking | null | measured | R1 | null | null | null | null | accepted | Instrument-reported results; repeated setpoints retained as rows, not independent experiments. | null | fsri:PUF_Mattress_Pad_HFM_Wet_HeatCapacity_220602_R1.tst:si:3 | License/reuse permission not established; local research evidence only | 0149187890d7e0ccfd7da2dc89228ffd9b4fdc57a66e1e36deeb6bc5c8fd8379 | 1 | not_reported_in_linked_identity | |||||
0c54bafebcf7f7a08b1d216ea8fec2340f4714d740c320cca069e2b8a7da8397 | 293261c992f887fd407c7246c776f9d6192d561d3ffc44bc671e66834c7cd9f2 | patents | data/raw/94ab98c6665420ca7e2cf5b773370697ef59005b2fcc647a776ecd472cef1ec5.bin | 94ab98c6665420ca7e2cf5b773370697ef59005b2fcc647a776ecd472cef1ec5 | US9455432B2:Ex. 1 | thermal_shrinkage | % MD Shrinkage @ 105° C. | 17.6 | % | 17.6 | % | https://patents.google.com/patent/US9455432B2/en | null | TABLE 1 | null | 15 | 2 | patent_html_table | separator-v32 | null | null | PE/PP | reviewed_sample_link | [{"locator": "p-0034", "text": "Various thickness hybrid laminated membranes were prepared by laminating wet process PE and dry process PP of different thicknesses. A two-fold improvement in puncture strength was observed when comparing Example 3 which has a puncture strength of 812 gf compared to CE 2 which has a punc... | null | bilayer | null | null | null | separator | not_reported | null | null | null | reported | 105 | exposure | null | null | MD | Patent experimental protocol p-0040 | Shrinkage is measured at two temperatures by placing a sample in an oven at 105 deg C. for one hour and placing a second sample in an oven at 120 deg C. for one hour. Shrinkage is measured in both machine direction (MD) and transverse direction (TD) and is reported as a % MD shrinkage and % TD shrinkage. | null | measured | null | null | null | null | null | accepted | Publication US9455432B2; Ex. 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p-0034 | p-0035 | 51528443 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 be677e3d6cfd7359f0218cf890c7ac8ba3a15d077766a8d74bba9b70173eb254; current SHA256 identifies sanitized bytes. | 014f37304f51cfc0fb0d169af6b64bdd6aa0462c75b17b6600dd8d19e58fba42 | 1 | not_reported_in_linked_identity | |||||
cf8029adaf6ef5f5b405bd69ac5d697c5fe5b46002ad2c227f46a509a1346870 | 34f9e0d8510703b6169de3622d952b0dc5751d58118b180c3620dcf9d048873e | patents | data/raw/36286c1618ed5ec12d2254c2c6e034d20d4da865d2a3cb9507cd262f011f6df9.bin | 36286c1618ed5ec12d2254c2c6e034d20d4da865d2a3cb9507cd262f011f6df9 | US7807287B2:Example 9 | porosity | Porosity (%) | 37.9 | % | 37.9 | % | https://patents.google.com/patent/US7807287B2/en | null | TABLE 1 | null | 162 | 2 | patent_html_table | separator-v32 | null | null | null | recipe_reference_not_linked | [{"locator": "num:p-0158", "text": "A first polyolefin solution was prepared in the same manner as in Example 1 except for using only HDPE as the polyethylene, and a second polyolefin solution was prepared in the same manner as in Example 1 except using the propylene homopolymer used in Example 3 as the polypropylene. ... | Referenced sample recipe has not been resolved: Example 1, Example 2 | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0171 | (3) Porosity (%) Measured by a weight method. | null | measured | null | null | null | null | null | accepted | Publication US7807287B2; Example 9; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 37890196 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 bbbf022a6e1678dded7aec76355e851f69ed8d8784b147cdd694ecafd69d304c; current SHA256 identifies sanitized bytes. | 016333fe2ea068d3e674b8b8f00015c1550e6e4f1bda3ed617c95dcbcac495a1 | 1 | not_reported_in_linked_identity | HDPE | ||||
3c115489b505eed6462461bb075fa1febc5498d8c4ea98ac4a50f6debaec1e50 | 3ca677c0f442efb15a1209e35cf1c61aa9c33e2a0915d1b160baf53ff222af3e | patents | data/raw/d0343cdc947553af700e941b1b000c1ef32923da78ee9520d0c0948d2c24bf47.bin | d0343cdc947553af700e941b1b000c1ef32923da78ee9520d0c0948d2c24bf47 | US20090134538A1:Example 7 | shutdown_response_time | Shutdown Speed (sec) | 15 | sec | 15 | s | https://patents.google.com/patent/US20090134538A1/en | null | TABLE 2 | null | 63 | 4 | patent_html_table | separator-v32 | null | null | null | recipe_reference_not_linked | [{"locator": "p-0165", "text": "A polypropylene melt was prepared in the same manner as in Example 5. The polypropylene melt was extruded from a T die attached to a tip end of a double-screw extruder, and cooled while taking off by a cooling roll controlled at 0° C., to form a polypropylene sheet. The polypropylene she... | Referenced sample recipe has not been resolved: Example 1, Example 3, Example 5 | null | null | null | null | separator | not_reported | null | null | null | reported | 135 | exposure | null | null | unspecified | Patent experimental protocol p-0153 | (9) Shutdown Speed Each multi-layer, microporous membrane was heat-treated by contact with a plate controlled at 135° C. for various periods of time and then measured with respect to air permeability. A time period (second) until the air permeability reached 100,000 seconds/100 cm 3 (converted to the value of 20-μm thi... | null | measured | null | null | null | {"canonical_unit": "s", "unit_alias": "sec"} | null | accepted | Publication US20090134538A1; Example 7; printed unit: sec. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed conditions: {"basis": "explicit_exposure_temperature", "metadata": {"temperature_C": 135.0, "temperature_role": "exposure"}, "previous_observation_id": "b64ac9cc8... | 37962566 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 b4e9cec5353afc839c29d236d8886811cddbe10d4e285ee76c450c2c8550b99f; current SHA256 identifies sanitized bytes. | 01668bc54c71483c68737324e87936bc3dc17ab172e663b463002e78d08f904e | 1 | not_reported_in_linked_identity | |||||
1a47276785c26bd39f4760504a297bb9efe15567a6936e227d5c0f56bc538ea7 | 259f24a1f72e2ecd04a40e815e11b560401b1320fb7fe665c967c5da7d8a8494 | patents | data/raw/805532f295c89cb5d754df8ad91c5c012aab7b6e91643d5a874871c9c7510bfb.bin | 805532f295c89cb5d754df8ad91c5c012aab7b6e91643d5a874871c9c7510bfb | US20100069596A1:Comparative Example 2 | thickness | Average Thickness (μm) | 19.7 | μm | 19.7 | um | https://patents.google.com/patent/US20100069596A1/en | null | TABLE 1 | null | 75 | 3 | patent_html_table | separator-v32 | null | null | PE | explicit_composition_table | [{"locator": "TABLE-US-00001", "text": "TABLE 1 No. Example 1 Example 2 Example 3 Example 4 Example 5 Resin Composition PE Composition UHMWPE Mw (1) 2.5 × 10 6 2.5 × 10 6 2.5 × 10 6 2.5 × 10 6 2.5 × 10 6 % by mass 30 30 30 20 20 HDPE Mw (1) 2.8 × 10 5 2.8 × 10 5 2.8 × 10 5 2.8 × 10 5 3.0 × 10 5 % by mass 70 70 70 80 80... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0139 | (1) Average Thickness (μm) The thickness of the microporous polyethylene membrane was measured at a 5-mm interval over a width of 30 cm by a contact thickness meter, and the measured thickness was averaged. | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Publication US20100069596A1; Comparative Example 2; printed unit: μm. Example identity and experimental protocol retained; no processing temperature inferred. | 38067215 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 6e1a8a735ab964eb91c750798ddce1675420112bc940e3d02e2e30acfde148b9; current SHA256 identifies sanitized bytes. | 016934d578167de9ea893c20f4c539e0dabe5b8185471929a44ed751fb63663c | 2 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
9cfe67bf1673b8a98dc9522f4097e7653222eba66d57e5439cd6d2c0fbc3e0b3 | 92c79112b84d275507fb07ff9005600706ea4d98905679cb93704722a04378c5 | fsri | data/runs/2026-10-26_source_probe_fsri/raw/a167a6e57593aed30acae0833ea4bddd8bafeb52d6e4d7d5f0a4fd00552aa50f.tst | a167a6e57593aed30acae0833ea4bddd8bafeb52d6e4d7d5f0a4fd00552aa50f | Black_PMMA_HFM_Dry_conductivity_211116_R2.tst | thermal_conductivity | conductivity | 0.1513 | W/(m K) | 0.1513 | W/(m K) | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/Black_PMMA/HFM/Black_PMMA_HFM_Dry_conductivity_211116_R2.tst | null | Results Table -- SI Units | null | Black_PMMA_HFM_Dry_conductivity_211116_R2.tst:row 3 | null | fsri_hfm_si | separator-v32 | null | null | Black_PMMA | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "Results Table -- SI Units", "source_file": "data/runs/2026-10-26_source_probe_fsri/raw/a167a6e57593aed30acae0833ea4bddd8bafeb52d6e4d7d5f0a4fd00552aa50f.tst", "source_sha256": "a167a6e57593aed30acae0833ea4bddd8bafeb... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 15.01 | measurement | null | null | through-plane | TA Instruments FOX HFM; SI results | FSRI Dry; ambient/unconditioned Wet is not electrolyte soaking | null | measured | R2 | null | null | null | null | accepted | Instrument-reported results; repeated setpoints retained as rows, not independent experiments. | null | fsri:Black_PMMA_HFM_Dry_conductivity_211116_R2.tst:si:3 | License/reuse permission not established; local research evidence only | 01751b770633d281848e83cda8a3ee9d0b8bb7e5606c0ff6c066ed61351fc5b0 | 1 | not_reported_in_linked_identity | |||||
a7a76ae343be8dd35c1e88bd6a9b4bbae286563824f24a3af5dfe43b2d39d970 | 01a4614f704c467ad91a5daf48395e5bbb83facbe68d96190d3471e495f71bc2 | patents | data/runs/2026-10-26_balanced/raw/fdafd96e1eb28fc94a1f6ee6dc6e86c62c78e5842cf3307415425cf7235cf193.bin | fdafd96e1eb28fc94a1f6ee6dc6e86c62c78e5842cf3307415425cf7235cf193 | US20210083253A1:Ex. 1 | thermal_shrinkage | MD/TD % Shrinkage 130° C./1 hour | 0.4 | % | 0.4 | % | https://patents.google.com/patent/US20210083253A1/en | null | TABLE 3 | null | 13 | 3 | patent_html_table | separator-v32 | null | null | null | sample_label_not_found | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | 130 | exposure | 60 | null | TD | Patent experimental protocol h-0014 | Thermal Shrinkage Shrinkage is measured by placing a coated test sample between two sheets of paper which is then clipped together to hold the sample between the papers and suspended in an oven. For the “130° C. for 1 hour” testing, a sample is placed in an oven at 130° C. for 1 hour. For the “150° C. for 10 minutes” t... | length | measured | null | null | null | null | null | accepted | Publication US20210083253A1; Ex. 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Printed MD/TD cell: 1.4/0.4. | 56284991 | null | License/reuse permission not established; local research evidence only | 0176fbdd86cca00aff9283aa1f6d18fd08758dfb381bcae20789bd01d67f83d0 | 1 | not_reported_in_linked_identity | |||||
e0954b478d2b4f88a659fc504e25fe3c3c0e256cc7d92edfe9b4cf45cafd0b78 | adcc230b3ae861011b931dc1a204f022ce09c766c33e1d6c1bfb7650418b8ec7 | patents | data/raw/1c72897d3aa9a7d75d98dbdcc1565b77743c2fedd81a70481944b3f637393d1d.bin | 1c72897d3aa9a7d75d98dbdcc1565b77743c2fedd81a70481944b3f637393d1d | US9419266B2:Example 4 | thickness | Thickness | 39 | μm | 39 | um | https://patents.google.com/patent/US9419266B2/en | null | TABLE 1 | null | 18 | 6 | patent_html_table | separator-v32 | null | null | null | not_linked_to_recipe | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0025 | (3) Measurement of Thickness The in-plane thickness of each porous polyolefin resin film was measured at unspecified 30 points thereof with a dial gauge 1/1000 mm. The average of the measured values is shown as the thickness thereof. | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Publication US9419266B2; Example 4; printed unit: μm. Example identity and experimental protocol retained; no processing temperature inferred. | 46580808 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 7d2919c28edf0b7f7a01792ef4b20ef6497308e520722af0a5bdc15d3ad02671; current SHA256 identifies sanitized bytes. | 01780fc27619278b581cfddf56f7152940b8a28fc01a29747eba73c6b7fdfbc7 | 1 | not_reported_in_linked_identity | |||||
d5ac80b778355f2b0bbb11c7c933e22e11e80b01145e403ca127b3f5d5a49590 | 2364a7f699366a817ed16c670d97f94facd8f491c3435e77e6ecba182d157399 | patents | data/raw/4e4214bcfefc40ada40700d0549b1c7917ead2322bf16f6bbd54e391aa5c4ca3.bin | 4e4214bcfefc40ada40700d0549b1c7917ead2322bf16f6bbd54e391aa5c4ca3 | US20090092893A1:Example 3 | porosity | Porosity (%) | 48.5 | % | 48.5 | % | https://patents.google.com/patent/US20090092893A1/en | null | TABLE 1 | null | 27 | 4 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p-0142", "text": "Dry-blended were 100 parts by mass of (i) a polyethylene (PE) composition comprising 5% by mass of ultra-high-molecular-weight polyethylene (UHMWPE) having a weight-average molecular weight (Mw) of 1.5×10 6 and a molecular weight distribution (Mw/Mn) of 8, and (ii) 95% by mass of high-de... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0067 | (3) Porosity (%) Measured by a weight method. | null | measured | null | null | null | null | null | accepted | Publication US20090092893A1; Example 3; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 40523543 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 94cb6922d5d234b78751c768de735129dc02e29a5246fe0ad5963668b347aa20; current SHA256 identifies sanitized bytes. | 017fabb771d282e1b93be34c9a6547c949156711f6efb5791dc023e4569bfb4b | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
10961deff98e22e713660b95c362610d27a179a63f742ddd1d464426beac7328 | 26d7bd4bf0703b034da14449c125b108e2f9e76034c26859f5120ad8a2fd024d | patents | data/raw/731c0b6804a5f7b4d5d3b86e3282a4a302b444c8786952a56c9b6d684b0d29c9.bin | 731c0b6804a5f7b4d5d3b86e3282a4a302b444c8786952a56c9b6d684b0d29c9 | US20130034777A1:Comparative Ex 1 | porosity | Porosity % | 37.5 | % | 37.5 | % | https://patents.google.com/patent/US20130034777A1/en | null | TABLE 1 | null | 29 | 2 | patent_html_table | separator-v32 | null | null | null | not_linked_to_recipe | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0112 | Porosity is measured by a weight method using the formula: Porosity %=100×(w2−w1)/w2, wherein “w1” is the actual weight of film and “w2” is the assumed weight of 100% polyethylene. | null | measured | null | null | null | null | null | accepted | Publication US20130034777A1; Comparative Ex 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 40651718 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 828327d7175c09a4903e8b2257fae142b33a33b622e556b00493a6b6115947b5; current SHA256 identifies sanitized bytes. | 01813d3da4ce7d536d0ebd6e4502c0bc2c25fa3b86160fdb6c6d127d95f4f19d | 1 | not_reported_in_linked_identity | |||||
0532ffb5c4e6d85f06c3f4f6ce2874591d48799be58073a0add5a5aca411eed9 | 1377fc49cc188be3568757283f01757ac545081b8454b408f060658736b9f1d6 | patents | data/runs/2026-10-19_expansion/raw/78fc83b885911a313b35805edc6a46500e6c3f29a8aeb5ca9a46ba9c8109181a.bin | 78fc83b885911a313b35805edc6a46500e6c3f29a8aeb5ca9a46ba9c8109181a | EP3181621A1:Comparative Example 2 | pore_size | TMA Pore size Maximum pore size (µm) | 0.038 | µm | 0.038 | um | https://patents.google.com/patent/EP3181621A1/en | null | table_3 | null | 11 | 8 | patent_html_table | separator-v32 | null | null | PE | reviewed_sample_link | [{"locator": "p0072", "text": "A polyethylene composition consisting of 30 wt.% of a PE 1 (ultrahigh molecular weight polyethylene, weight average molecular weight (Mw): 2.89 × 10 6 , molecular weight distribution (Mw/Mn): 5.28) as an ultrahigh molecular weight polyethylene and 70 wt.% of a PE2 (high-density polyolefin... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h0021 | 9. Maximum pore size and peak top pore size The maximum pore size and the peak top pore size of the microporous membrane were calculated as follows. First, the relationship between air pressure and air flow rate was measured for a sample in a dry state and a sample in a wet state prepared by filling the fine pores with... | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u00b5m"} | null | accepted | Publication EP3181621A1; Comparative Example 2; printed unit: µm. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p0072 | p0080 | p0079 | 55304161 | null | License/reuse permission not established; local research evidence only | 018d51c13b247d8160b9ec8db42517a8866c7fe402f847d15c2c6ef018ce4de3 | 3 | not_reported_in_linked_identity | UHMWPE | ||||
1f2f617f8498a62d2f92ce1f5f4a3e2a20ca1506066edd3996f15691dd35c9a9 | c0cf52c161f30b928bc9085205aafa86c41669a4e3583c19b0607866ff44d5ba | patents | data/runs/2026-10-26_balanced/raw/b06535949313e1ab5f623dc7a741424e980ef5d0bf55f99beddb367f1a152680.bin | b06535949313e1ab5f623dc7a741424e980ef5d0bf55f99beddb367f1a152680 | US20220389203A1:Example 10 | porosity | Porosity % | 36 | % | 36 | % | https://patents.google.com/patent/US20220389203A1/en | null | TABLE 1 | null | 150 | 6 | patent_html_table | separator-v32 | null | null | PE/PP | inherited_recipe | [{"locator": "p-0228", "text": "(A) A high-density polyethylene (PE5) having My of 700000 and polydispersity (Mw/Mn) of 7.9 in an amount of 45% by weight was dry-blended with a high-density polyethylene (PE2) having My of 250000 and polydispersity (Mw/Mn) of 7.2 in an amount of 45% by weight and a homopolypropylene (PP... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0029 | [Porosity (%)] A 10 cm×10 cm square sample was cut from the polyolefin microporous membrane, the volume (cm 3 ) and mass (g) thereof were determined, and these values and the density (g/cm 3 ) were used in the following formula: Porosity (%)=(volume−mass/density of mixed composition)/volume×100 The density of the mixed... | null | measured | null | null | null | null | null | accepted | Publication US20220389203A1; Example 10; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 75437241 | null | License/reuse permission not established; local research evidence only | 019f69b63e62011730e6f987e561b9b70defce041c1701841a46d0a17cc387bf | 1 | not_reported_in_linked_identity | HDPE | ||||
80c46ab184645f9030be263c59608394960bc85d8ecf4e3a1b58e294e81d1755 | 6fabff39b8e5ce21ce89da927a586f7f83d1d196d6fca54fbce5132c23f16772 | patents | data/runs/2026-10-26_balanced/raw/89182a941a872e260a105859aadbdf0b739ce325e27e12b205836f489a4cebff.bin | 89182a941a872e260a105859aadbdf0b739ce325e27e12b205836f489a4cebff | EP4578899A1:Ex. 2 | pore_size | Average pore size (nm) | 27.9 | nm | 0.0279 | um | https://patents.google.com/patent/EP4578899A1/en | null | table_1 | null | 3 | 6 | patent_html_table | separator-v32 | null | null | null | changed_recipe_needs_link | [{"locator": "p0096", "text": "A polyolefin microporous membrane was manufactured in the same manner as in Example 1, except that a polyolefin resin including 20 wt% of the polyethylene resin and 80 wt% of the polypropylene resin was used instead of the polyolefin resin of Example 1, and the results are listed in Table... | Inherited recipe changes material composition; exact resulting recipe not yet linked | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h0015 | 8. Average pore size (nm) The average pore size was measured from a porometer (CFP-1500-AEL available from PMI) in accordance with ASTM F316-03. The average pore size was measured by a half dry method, and a Galwick solution (surface tension: 15.9 dyne/cm) provided for measuring a pore size by PMI was used. | null | measured | null | null | null | {"offset": 0, "scale": 0.001} | null | accepted | Publication EP4578899A1; Ex. 2; printed unit: nm. Example identity and experimental protocol retained; no processing temperature inferred. | 94083464 | null | License/reuse permission not established; local research evidence only | 01a396894ba1f1a5d38aab1098a959d2aa12ac83198b4eb063ecc671aed91822 | 1 | not_reported_in_linked_identity | |||||
64d4cf3d41c211c3ce96b9871774ac15dbca3f6cdc394f24ba2b5492c709f100 | 7163dffaf12133c4328dfa86357a9981733d4f1551567ce0baf2b4ca2cd4aa4d | patents | data/raw/32f9dbf6183f1f3f566d8dc5c24f56951854cb79e080d9e7549ad60b27fcf7ae.bin | 32f9dbf6183f1f3f566d8dc5c24f56951854cb79e080d9e7549ad60b27fcf7ae | US20130164598A1:Example 6 | meltdown_temperature | Meltdown Temperature (° C.) | 177.0 | ° C. | 177 | C | https://patents.google.com/patent/US20130164598A1/en | null | TABLE 1 | null | 66 | 2 | patent_html_table | separator-v32 | null | null | null | not_linked_to_recipe | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0042 | Meltdown Temperature (as Measured by Membrane Rupture) Meltdown temperature is measured as follows. A sample of the microporous membrane measuring 5 cm×5 cm is fastened along its perimeter by sandwiching the sample between metallic blocks each having a circular opening of 12 mm in diameter. The blocks are then position... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0 C."} | null | accepted | Publication US20130164598A1; Example 6; printed unit: ° C.. Example identity and experimental protocol retained; no processing temperature inferred. | 45567640 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 4619d06d55b4e841d7ef07abf1d0a6a97bca387ac87fab12e8dacb5208067f20; current SHA256 identifies sanitized bytes. | 01a4a0909c9e843f52b228a1c94847e65b92d3e48e37be380f5c821e4136b634 | 2 | not_reported_in_linked_identity | |||||
e0b656b63bb6d59a810caefda500fc9604bc897d52ae36a665cc74ffb9d26a45 | 090bb3b14b35b18ee98ebe0f958b74ab0a50c441a7172adb31f57bb99319155e | patents | data/raw/0229257243885beb5a70ef860f76b2f3a9daa3c63bbbf2ee3326d01930e47b44.bin | 0229257243885beb5a70ef860f76b2f3a9daa3c63bbbf2ee3326d01930e47b44 | US8026005B2:Comp. Ex. 1 | porosity | Porosity (%) | 38 | % | 38 | % | https://patents.google.com/patent/US8026005B2/en | null | TABLE 1 | null | 129 | 3 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "num:p-0132", "text": "Dry-blended were 100 parts by mass of (i) a polyethylene (PE) composition comprising 5% by mass of ultra-high-molecular-weight polyethylene (UHMWPE) having a weight-average molecular weight (Mw) of 1.5×10 6 and a molecular weight distribution (Mw/Mn) of 8, and (ii) 95% by mass of hig... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0154 | (3) Porosity (%) Measured by a weight method. | null | measured | null | null | null | null | null | accepted | Publication US8026005B2; Comp. Ex. 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 38581278 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 830ff0c37fe20fd65f06a5cc34d812055b65d60e441b58f4154396e7bd65a73e; current SHA256 identifies sanitized bytes. | 01acc411bca95a695ca2fffe61a79e5ceb7b322b5dabcde8b4a04c36e9d3c375 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
b8d3d5f186274e3788a7007d731d65e52c82f50eed96d887f0f316341f60c6f5 | 0dea6d581abd14726def4375f67162783f2cf13a7698bac96c0eda96f68e1fbb | patents | data/runs/2026-10-23_balanced/raw/ca3748f4f0a6f12d7edbdacd3123d9599826f0f0ae5f0bfb3990072474fa9dec.bin | ca3748f4f0a6f12d7edbdacd3123d9599826f0f0ae5f0bfb3990072474fa9dec | EP4040589A1:Comp. Ex.12 | tensile_strength | Tensile strength (kgf/cm 2 ) | 1450 | kgf/cm 2 | 142.196425 | MPa | https://patents.google.com/patent/EP4040589A1/en | null | table_3 | null | 10 | 9 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p0137", "text": "A polyethylene porous film (available from Toray, porosity: 45%) having a thickness of 9 µm was prepared as a polyolefin porous substrate."}, {"locator": "p0143", "text": "In this manner, a crosslinked separator for a lithium secondary battery comprising a crosslinked polyolefin porous su... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h0037 | (6) Evaluation of Tensile Strength in Machine Direction and Transverse Direction and Change in Tensile Strength in Machine Direction A specimen having a size of 100 mm × 15 mm was prepared. According to ASTM D882, the specimen was drawn in each of the machine direction and the transverse direction at a rate of 50 mm/mi... | null | measured | null | null | null | {"offset": 0, "scale": 0.0980665} | null | accepted | Publication EP4040589A1; Comp. Ex.12; printed unit: kgf/cm 2 . Example identity and experimental protocol retained; no processing temperature inferred. | 75849009 | null | License/reuse permission not established; local research evidence only | 01c10601661ae106f98afd95edb41702baf9643023a429fad42fa9e9cb7802a0 | 1 | not_reported_in_linked_identity | |||||
e9442654fc94c7babc6e74abb58d4b494c6da7bfd06d479eb157995207b31b4c | f2b5be5d8c3eedd711149c606efd31f643131432f96dcee7d11bb0fdb4139543 | celgard | data/raw/a8638dedfabf6bd150184d292afb6a4dc5d5768dfdb12ac612ca4fd7b8f95fcb.pdf | a8638dedfabf6bd150184d292afb6a4dc5d5768dfdb12ac612ca4fd7b8f95fcb | celgard_3501 | thickness | Thickness | 25 | μm | 25 | um | https://www.celgard.com/storage/components/3501_com_data_2026-01.pdf | 1 | 1 | null | 3 | 3 | pymupdf.find_tables | separator-v32 | Celgard | 3501 | PP | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "1", "source_file": "data/raw/a8638dedfabf6bd150184d292afb6a4dc5d5768dfdb12ac612ca4fd7b8f95fcb.pdf", "source_sha256": "a8638dedfabf6bd150184d292afb6a4dc5d5768dfdb12ac612ca4fd7b8f95fcb"}] | Material supplied by source adapter or reviewed import; see source coordinates and notes | monolayer | surfactant | null | polyolefin separator | separator | not_reported | null | null | null | typical | null | unknown | null | null | unspecified | null | Thickness | null | unknown | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Manufacturer table; source unit as printed: μm. Typical specifications do not establish an experimental measurement temperature. | null | null | License/reuse permission not established; local research evidence only | 01c5bdee1cf29696784e8637a0613fe50fec04f493724bf6fe4b577d30c5ac1d | 1 | not_reported_in_linked_identity | |||||
8baed0c98c5071e75d99a2db17336dc5e296965766c691b3fb34fe26191a5a2a | 7812d3f3990816ce9880da04a5babed76e2c74d8916ef4991c112ec7413baa31 | manual | data/raw/f0e179557f65816dc6eb4bc3fe3e331b3bd593a72f5d28c51895994fcd05ef5a.csv | f0e179557f65816dc6eb4bc3fe3e331b3bd593a72f5d28c51895994fcd05ef5a | PMC10680142:PLI(0)@PP | ionic_conductivity | ionic_conductivity | 4.76304424054932e-05 | S/cm | 0.004763 | S/m | https://www.ebi.ac.uk/europepmc/webservices/rest/PMC10680142/fullTextXML | null | null | 3f | 11 | null | manual_structured_import | separator-v32 | null | null | PEO/PP | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "11", "source_file": "data/raw/f0e179557f65816dc6eb4bc3fe3e331b3bd593a72f5d28c51895994fcd05ef5a.csv", "source_sha256": "f0e179557f65816dc6eb4bc3fe3e331b3bd593a72f5d28c51895994fcd05ef5a"}] | Material supplied by source adapter or reviewed import; see source coordinates and notes | PP support infiltrated with PEO/LiTFSI/ionic-liquid electrolyte | PEO/LiTFSI/ionic liquid | null | null | separator | not_reported | LiTFSI | 1-ethyl-3-methylimidazolium bis(trifluoromethanesulfonyl)imide ionic liquid; PEO matrix | null | reported | 50 | measurement | null | null | unspecified | AC impedance; stainless-steel blocking electrodes; 5 mV; 0.1 Hz-1 MHz; chamber stabilized 30 min | IL loading 0 wt%; native Figure 3f marker; calibration uncertainty 2 pixels | null | digitized_estimate | null | 021d16576ff3892720bbf6099dd29efc423357c846cfcddefb1e85d04e152072 | 0.001247 | {"offset": 0.0, "scale": 100.0} | null | accepted | Primary XML data/runs/2026-10-30_temperature_expansion/raw/2045a673e943da3c2706a69d01e91b231128941d5abfc82f740c53ce324b3a02.bin; SHA256 2045a673e943da3c2706a69d01e91b231128941d5abfc82f740c53ce324b3a02. Solid polymer/ionic-liquid electrolyte-filled support; not pure PP or liquid-soaked neat membrane. Figure SHA256 b7864... | null | null | Primary RSC paper CC BY-NC 3.0; derived marker estimates retain source attribution and uncertainty. | 01d1d3ff65705f5c6338d1db7a373f177dc3de2dffd9167afad9f5c9fd68fb06 | 1 | not_reported_in_linked_identity | |||||
931dfba31e95dba66369312d11d569fdf8be3a21433273f8e94a62132b85e09c | 3297d03f9b6c615033b08b847a151fa041371df5eaaa2da6a69898a32833c47f | fsri | data/runs/2026-10-30_thermal/raw/854c0a11f1d4ea95762124db2ad0a105a0d333c0f54e26b044a3dd27abc8c81d.csv | 854c0a11f1d4ea95762124db2ad0a105a0d333c0f54e26b044a3dd27abc8c81d | LDPE_STA_N2_30KData_210908_R3 | sta_mass_percent | Mass(subtr.2)/% | 100.04134 | % | 100.04134 | % | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/LDPE/STA/N2/30K_min/LDPE_STA_N2_30KData_210908_R3.csv | null | null | null | LDPE_STA_N2_30KData_210908_R3.csv:CSV row 2010 | Mass(subtr.2)/% | fsri_sta_native_csv | separator-v32 | null | null | LDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "LDPE_STA_N2_30KData_210908_R3.csv:CSV row 2010", "source_file": "data/runs/2026-10-30_thermal/raw/854c0a11f1d4ea95762124db2ad0a105a0d333c0f54e26b044a3dd27abc8c81d.csv", "source_sha256": "854c0a11f1d4ea95762124db2ad... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 250.02 | measurement | null | 30 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R3 | fsri:STA:LDPE_STA_N2_30KData_210908_R3 | null | null | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 a... | null | fsri:STA:LDPE_STA_N2_30KData_210908_R3:row:2010:sta_mass_percent | License/reuse permission not established; local research evidence only | 01d81b403e936051088c1d974916d6be6330c97c80a6fa0da01ef2261ba76ffc | 1 | LDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "LDPE", "labels": ["LDPE"]}, {"field": "sample_id", "text": "LDPE_STA_N2_30KData_210908_R3", "labels": ["LDPE"]}] | LDPE | ||
50b8be99b27e2458cd2f72666f97ab5440a07350deb176b8f23528e356b28216 | 1ff65f333b21d45df1863b67ba6269454a8c1e7fca9f90d809d103ae85a7ec4d | patents | data/runs/2026-10-23_balanced/raw/508d5ef59458dab75be7d149814e884a16bdbe2d616b987765f5c7ea66aadc0a.bin | 508d5ef59458dab75be7d149814e884a16bdbe2d616b987765f5c7ea66aadc0a | EP2728645B1:Example 2 | thermal_shrinkage | MD THERMAL SHRINKAGE RATIO (%) | 0.88 | % | 0.88 | % | https://patents.google.com/patent/EP2728645B1/en | null | table_1 | null | 4 | 11 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p0047", "text": "A polyethylene (PE) microporous membrane having a thickness of 10 µm and a porosity of 65% and an aqueous solution containing 95 mass% alumina (Al 2 O 3 ) particles and 5 mass% carboxymethylcellulose (CMC) evenly dispersed in water were prepared. The prepared aqueous solution was applied ... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 150 | exposure | null | null | MD | Patent experimental protocol h0050 | <Thermal shrinkage Test: Evaluation of Thermal shrinkage Resistance> Each separator was cut into 20 cm by 20 cm, and the dimension thereof in the MD direction was measured. The measurement result thereof was set to an initial dimension. Subsequently, the separator was left in a constant-temperature bath at 150°C. An ho... | null | measured | null | null | null | null | null | accepted | Publication EP2728645B1; Example 2; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 47424013 | null | License/reuse permission not established; local research evidence only | 01e4d145f788821c1f457d84cfb2f99dac6a35fbeac06bde4f7e5216c29e2738 | 1 | not_reported_in_linked_identity | |||||
f0ed36d5de1074ae6bedde876a18bb008822065d2a8ec0ed9b8c6946f342cde3 | f6db710737d25d249c485deaae815ddb24eebe12f7e967dcc5238eeea93797e2 | fsri | data/runs/2026-10-30_thermal/raw/e05bf4105fabb295211527538572b21f2c30d1491328485544c1c99290040853.csv | e05bf4105fabb295211527538572b21f2c30d1491328485544c1c99290040853 | HDPE_STA_N2_30KData_21109_R3 | mass_specific_heat_flow | DSC(subtr.2)/(mW/mg) | 0.4085 | mW/mg | 408.5 | W/kg | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/HDPE/STA/N2/30K_min/HDPE_STA_N2_30KData_21109_R3.csv | null | null | null | HDPE_STA_N2_30KData_21109_R3.csv:CSV row 108 | DSC(subtr.2)/(mW/mg) | fsri_sta_native_csv | separator-v32 | null | null | HDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "HDPE_STA_N2_30KData_21109_R3.csv:CSV row 108", "source_file": "data/runs/2026-10-30_thermal/raw/e05bf4105fabb295211527538572b21f2c30d1491328485544c1c99290040853.csv", "source_sha256": "e05bf4105fabb295211527538572b... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 59.982 | measurement | null | 30 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R3 | fsri:STA:HDPE_STA_N2_30KData_21109_R3 | null | {"offset": 0.0, "scale": 1000.0} | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 9... | null | fsri:STA:HDPE_STA_N2_30KData_21109_R3:row:108:mass_specific_heat_flow | License/reuse permission not established; local research evidence only | 01e7d91303269cba4baac0738f1442d622c6f6987acc54d965a132ea73259adc | 1 | HDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "HDPE", "labels": ["HDPE"]}, {"field": "sample_id", "text": "HDPE_STA_N2_30KData_21109_R3", "labels": ["HDPE"]}] | HDPE | ||
ed5c1715121fac1794e092b62bfb9e3e4f179e73652036dbe9933dbec88c95f2 | 29cabffb9ca93599452a8b179f5ba540fee9a0d8fa3dff1fd0315fff4e0da092 | patents | data/raw/70a2f68b8c64dc53e8564279929c46c02198f3ec833411a676d59ae1b349d7a0.bin | 70a2f68b8c64dc53e8564279929c46c02198f3ec833411a676d59ae1b349d7a0 | US11242440B2:Example 15 | thickness | Physical Thickness (μm) | 10 | μm | 10 | um | https://patents.google.com/patent/US11242440B2/en | null | TABLE 2 | null | 53 | 7 | patent_html_table | separator-v32 | null | null | PE | explicit_recipe | [{"locator": "p-0151", "text": "Polyethylene was synthesized using the polyethylene synthesis catalyst listed in any one of Tables 1 to 4 (represented as “synthesis catalyst” in the tables) and an ethylene monomer. As shown in Tables 1 to 4, in each Example, two types of polyethylenes wherein one polyethylene type was ... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 23 | measurement | null | null | unspecified | Patent experimental protocol h-0027 | (3) Membrane Thickness (μm) The membrane thickness was measured at a room temperature of 23° C. using a micro thickness gauge (type KBM, manufactured by Toyo Seiki Co., Ltd.). | null | measured | null | null | null | {"canonical_unit": "um", "unit_alias": "\u03bcm"} | null | accepted | Publication US11242440B2; Example 15; printed unit: μm. Example identity and experimental protocol retained; no processing temperature inferred. | 63674906 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 28f3184b80b10819376843b18950734bae6c8d3770f7535bfd5543a02504f063; current SHA256 identifies sanitized bytes. | 01f1006458de23b104ab4f8ced6845cc13e567d64ee4cf81a644714c64d9a4a3 | 1 | not_reported_in_linked_identity | |||||
0be1162475dc4721ba30790d0d332d94b54f2a945c303d598a84caf27e3c1130 | 3297d03f9b6c615033b08b847a151fa041371df5eaaa2da6a69898a32833c47f | fsri | data/runs/2026-10-30_thermal/raw/854c0a11f1d4ea95762124db2ad0a105a0d333c0f54e26b044a3dd27abc8c81d.csv | 854c0a11f1d4ea95762124db2ad0a105a0d333c0f54e26b044a3dd27abc8c81d | LDPE_STA_N2_30KData_210908_R3 | mass_specific_heat_flow | DSC(subtr.2)/(mW/mg) | 1.22386 | mW/mg | 1,223.86 | W/kg | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/LDPE/STA/N2/30K_min/LDPE_STA_N2_30KData_210908_R3.csv | null | null | null | LDPE_STA_N2_30KData_210908_R3.csv:CSV row 760 | DSC(subtr.2)/(mW/mg) | fsri_sta_native_csv | separator-v32 | null | null | LDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "LDPE_STA_N2_30KData_210908_R3.csv:CSV row 760", "source_file": "data/runs/2026-10-30_thermal/raw/854c0a11f1d4ea95762124db2ad0a105a0d333c0f54e26b044a3dd27abc8c81d.csv", "source_sha256": "854c0a11f1d4ea95762124db2ad0... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 125.02 | measurement | null | 30 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R3 | fsri:STA:LDPE_STA_N2_30KData_210908_R3 | null | {"offset": 0.0, "scale": 1000.0} | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 a... | null | fsri:STA:LDPE_STA_N2_30KData_210908_R3:row:760:mass_specific_heat_flow | License/reuse permission not established; local research evidence only | 01f129c76b140e9f223695259d8c15e1f4f917962183f46909bfe4f6341543a2 | 1 | LDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "LDPE", "labels": ["LDPE"]}, {"field": "sample_id", "text": "LDPE_STA_N2_30KData_210908_R3", "labels": ["LDPE"]}] | LDPE | ||
ab029a20c7225e06c75542c6eae806dbd25c189812948c4227b5223274f49cbb | 09fa8fa3c6f0a3830dbc392ee443226cad68bfa37094e23d3e0b64855d09b40d | patents | data/runs/2026-10-26_balanced/raw/c6e3235a64105dc264fd9a053e3a98612fe3cab5d6272a75a7cea48fef68fed2.bin | c6e3235a64105dc264fd9a053e3a98612fe3cab5d6272a75a7cea48fef68fed2 | US20060103055A1:Example 1 | porosity | Porosity (%) | 48 | % | 48 | % | https://patents.google.com/patent/US20060103055A1/en | null | TABLE 1 | null | 22 | 2 | patent_html_table | separator-v32 | null | null | PE | explicit_sample_description | [{"locator": "p-0134", "text": "45 Parts by weight of the same high-density polyethylene as described in Example 1 and 0.3 part by weight of 2,6-di-t-butyl-p-cresol were dry blended in a Henschel mixer and fed into a 35-mm twin-screw extruder. Then, 55 parts by weight of di(2-ethylhexyl) phthalate were introduced into ... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p-0086 | (2) Porosity A specimen 20 cm square was cut out of a microporous membrane and its volume (cm 3 ) and weight (g) were measured. From the results obtained, porosity (%) was calculated by the following equation: Porosity = 100 × ( 1 - weight ÷ ( density of resin × volume ) ) | null | measured | null | null | null | null | null | accepted | Publication US20060103055A1; Example 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 26435161 | null | License/reuse permission not established; local research evidence only | 0202fb49250fefd0866957c56d2d8494a264254a0bf461c7c9e241d488d84d86 | 1 | not_reported_in_linked_identity | HDPE | ||||
d1e36de8fb2d12cd7d3e746e38d12d9c7a9cc1207b7e9b926d3ba4654496f042 | 7efbc8b27ef7bfe5760a8975f6ee7d1c9a1a18addd66e246dd0069e8a8645eb3 | fsri | data/runs/2026-10-30_thermal/raw/b133713e0a2cf4f9cf988815fab21810e01059103b0ed12f14176d1a00dbe9a4.csv | b133713e0a2cf4f9cf988815fab21810e01059103b0ed12f14176d1a00dbe9a4 | PET_STA_N2_10KData_210831_R3 | mass_specific_heat_flow | DSC(subtr.2)/(mW/mg) | 0.31279 | mW/mg | 312.79 | W/kg | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/PET/STA/N2/10K_min/PET_STA_N2_10KData_210831_R3.csv | null | null | null | PET_STA_N2_10KData_210831_R3.csv:CSV row 610 | DSC(subtr.2)/(mW/mg) | fsri_sta_native_csv | separator-v32 | null | null | PET | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "PET_STA_N2_10KData_210831_R3.csv:CSV row 610", "source_file": "data/runs/2026-10-30_thermal/raw/b133713e0a2cf4f9cf988815fab21810e01059103b0ed12f14176d1a00dbe9a4.csv", "source_sha256": "b133713e0a2cf4f9cf988815fab21... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 109.999 | measurement | null | 10 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R3 | fsri:STA:PET_STA_N2_10KData_210831_R3 | null | {"offset": 0.0, "scale": 1000.0} | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 2... | null | fsri:STA:PET_STA_N2_10KData_210831_R3:row:610:mass_specific_heat_flow | License/reuse permission not established; local research evidence only | 02157bc56bca5e9fa89d8e333aa4adbf3b4cc81c49ee2c3e3aa845ce0dab10b6 | 1 | not_reported_in_linked_identity | |||||
94b044648a34d61bff7fc18cc58e0dad824a3fa46aeb229e65c5ae94117e31ca | c0cdbb4ceb6dddb4e143f008fe074dbbe372b6a50d02e0997e25c04410d7480f | patents | data/runs/2026-10-26_balanced/raw/8da717f0dae15ad3bd29645f8cc180692133b341e89118eb62d723dbc6985873.bin | 8da717f0dae15ad3bd29645f8cc180692133b341e89118eb62d723dbc6985873 | EP3632972B1:Comparative Example 8 | porosity | Porosity | 79 | % | 79 | % | https://patents.google.com/patent/EP3632972B1/en | null | table_9 | null | 3 | 5 | patent_html_table | separator-v32 | null | null | PE/PP | explicit_composition_table | [{"locator": "css:html:nth-of-type(1) > body:nth-of-type(1) > search-app:nth-of-type(1) > article:nth-of-type(1) > section:nth-of-type(5) > div:nth-of-type(1) > ul:nth-of-type(1) > li:nth-of-type(148) > div:nth-of-type(1) > tables:nth-of-type(4) > patent-tables:nth-of-type(1) > table:nth-of-type(1)", "text": "Membrane ... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 23 | measurement | null | null | unspecified | Patent experimental protocol h0030 | (4)Porosity (%) A 10cm × 10cm square sample was cut out from the polyolefin microporous membrane, the volume (cm 3 ) and weight (g) of the sample were measured, and the porosity was calculated from these and the membrane density (g /cm 3 ) using the following equation: Porosity % = Volume − Weight / Membrane density / ... | null | measured | null | null | null | null | null | accepted | Publication EP3632972B1; Comparative Example 8; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed conditions: {"basis": "Source explicitly declares a physical-test temperature default; property-specific method checked for overrides. US20240079723 porosit... | 64396622 | null | License/reuse permission not established; local research evidence only | 02216666575a95318cac32ad9804cccbde47123cb25456440fe776d4404cd05e | 1 | not_reported_in_linked_identity | |||||
5a759557d39559e7ebdc656b86c1da3bea7edd215b71862f6386e5d48fccf573 | 901cc8cba1f625c352bd1c377ef0132fd7c6eae700248ef1c6c58decd076883b | patents | data/runs/2026-10-26_balanced/raw/eb99a789875b14233f7b4856b1fb821d72f954a7ee27859ccdac914f01081c4f.bin | eb99a789875b14233f7b4856b1fb821d72f954a7ee27859ccdac914f01081c4f | US20120034519A1:Ex. 5 | shutdown_temperature | Shutdown Temperature (° C.) | 128.5 | ° C. | 128.5 | C | https://patents.google.com/patent/US20120034519A1/en | null | TABLE 1 | null | 40 | 6 | patent_html_table | separator-v32 | null | null | PE | explicit_composition_table | [{"locator": "TABLE-US-00002", "text": "TABLE 1 No. Ex. 1 Ex. 2 Ex. 3 Ex. 4 Ex. 5 Ex. 6 Ex. 7 Ex. 8 Ex. 9 Resin Composition PE Composition First PE Mw 3.8 × 3.8 × 3.8 × 4.5 × 1.2 × 2.6 × 1.7 × 2.4 × 3.8 × 10 4 10 4 10 4 10 4 10 5 10 5 10 5 10 5 10 4 Mw/Mn 3.0 3.0 3.0 3.0 2.5 2.5 2.8 4.4 3.0 Tm(° C.) 125.8 125.8 125.8 1... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0026 | (c) Shutdown Temperature≦130.5° C. The microporous membrane's shutdown temperature is measured by the method disclosed in PCT publication WO2007/052663, which is incorporated by reference herein in its entirety. According to this method, the microporous membrane is exposed to an increasing temperature (5° C./minute beg... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0 C."} | null | accepted | Publication US20120034519A1; Ex. 5; printed unit: ° C.. Example identity and experimental protocol retained; no processing temperature inferred. | 42828625 | null | License/reuse permission not established; local research evidence only | 0223ca7ac5a6e333017c28cc3fd0caad2cfa406b68a7f2f4d656c7030798e5da | 1 | not_reported_in_linked_identity | |||||
ed97183399a031fdb90ccfaada5b14a9bd0d43214550861f18fa58e06f7b00a1 | 8083f5292d2e398779825c0437c7cf7329a3a95e82442d538b347e2773e852d5 | patents | data/raw/6ad9bcd2e9bc232fd67ce4fd4604c100aa62fbd3222e2ad2c16d68135e8f46a2.bin | 6ad9bcd2e9bc232fd67ce4fd4604c100aa62fbd3222e2ad2c16d68135e8f46a2 | US9431642B2:Example 2 | elongation | Tensile Rupture Elongation (%) MD/TD | 200 | % | 200 | % | https://patents.google.com/patent/US9431642B2/en | null | table_1 | null | 50 | 3 | patent_html_table | separator-v32 | null | null | PE/PP | inherited_recipe | [{"locator": "p-0158", "text": "Dry-blended were 100 parts by mass of a polyethylene composition comprising 20% by mass of ultra-high-molecular-weight polyethylene (UHMWPE) having a mass-average molecular weight (Mw) of 2.0×10 6 , and 80% by mass of high-density polyethylene (HDPE) having Mw of 3.5×10 5 , and 0.2 parts... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | MD | Patent experimental protocol p-0196 | (5) Tensile Rupture Strength and Tensile Rupture Elongation They were measured using a 10-mm-wide rectangular test piece according to ASTM D882. | null | measured | null | null | null | null | null | accepted | Publication US9431642B2; Example 2; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Printed MD/TD cell: 200/250. | 37668759 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 27ecf3bb50e45a2cbc55fca3eea7044db45bb8d851193a55f9bbf7a6a1cc0442; current SHA256 identifies sanitized bytes. | 022b87ccbd0596a52e0b561064522b1580b69e77026e735f9d6e0b3e23c771c9 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
2a7f812a07dc21c95d486f0752b5ee1e10265a1caeed8bbe7b4dffa73513ede5 | a07f50c2f4fc0d0d1bb15c3f2989217b80948e44fd0c0130e8484c635d9c3a4c | patents | data/runs/2026-10-26_balanced/raw/541f51645e14c190990407fd3e6b27e950b7f24b84d9e22899914bd4e40774a0.bin | 541f51645e14c190990407fd3e6b27e950b7f24b84d9e22899914bd4e40774a0 | EP2065432A1:Example 14 | porosity | Microporous membrane characteristics Porosity % | 52 | % | 52 | % | https://patents.google.com/patent/EP2065432A1/en | null | table_3 | null | 10 | 7 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p0100", "text": "14 parts by mass of high density polyethylene \"SH800\" (trademark, made by Asahi Kasei Chemicals Corporation) having a viscosity average molecular weight (Mv) of 270,000, 10 parts by mass of an ultra-high molecular weight polyethylene \"UH850\" (trademark, made by Asahi Kasei Chemicals C... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h0016 | (8) Porosity diameter ratio A porosity diameter ratio of a microporous membrane is represented by (surface porosity diameter)/(cross-section porosity ratio). For the surface porosity diameter of the microporous membrane, a long diameter and a short diameter of pores present per 5 cm × 5 cm of a scanning electron microg... | null | measured | null | null | null | null | null | accepted | Publication EP2065432A1; Example 14; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. | 39200499 | null | License/reuse permission not established; local research evidence only | 022c1ed38be828fc1ca8378d2346e841f5e45dbbbd4f724b7d494e252e59a922 | 1 | not_reported_in_linked_identity | HDPE/UHMWPE | ||||
dc2f2b37ffbc77cd8684b2f5ea9dfe73bbb32c1a51ca37b5b33953f802424469 | 479b953b2a76c95681c3f1f778b0fa62ecd1cde8bcbab83bc14112045d27273f | patents | data/runs/2026-10-26_balanced/raw/03fd5c0819300d0ed980f0c079109cac30d8e3d8b6d683b94e00357ea50f3483.bin | 03fd5c0819300d0ed980f0c079109cac30d8e3d8b6d683b94e00357ea50f3483 | EP4265670A1:Control example 3 | pore_size | Maximum pore size(nm) | 64 | nm | 0.064 | um | https://patents.google.com/patent/EP4265670A1/en | null | table_1 | null | 26 | 5 | patent_html_table | separator-v32 | null | null | null | not_linked_to_recipe | null | Sample label has no unique experimental-example mapping | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol p0061 | Maximum pore size: it is measured by using a narrow pore meter based on the bubble point method with nitrogen. | null | measured | null | null | null | {"offset": 0, "scale": 0.001} | null | accepted | Publication EP4265670A1; Control example 3; printed unit: nm. Example identity and experimental protocol retained; no processing temperature inferred. | 75195848 | null | License/reuse permission not established; local research evidence only | 022f44f65ed02992990a0c040a1dd24c464195d0fc9b8b98b8f2ad37b70ff8fb | 1 | not_reported_in_linked_identity | |||||
8c11eac85968106796ebf8f502b9be076d7955a8b1d99d22a5998aa72688436a | 41555b58c43f83ebb7fdb4cf30cf3d015b6c042e5b8bef1b2690a21c4ecc1abb | fsri | data/runs/2026-10-26_source_probe_fsri/raw/b6687789d92a123f97ef8442517d96981f19b38fe6e6740b90fb2e5ca95578de.tst | b6687789d92a123f97ef8442517d96981f19b38fe6e6740b90fb2e5ca95578de | PC_HFM_Wet_conductivity_210726_R2.tst | thermal_conductivity | conductivity | 0.1716 | W/(m K) | 0.1716 | W/(m K) | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/PC/HFM/PC_HFM_Wet_conductivity_210726_R2.tst | null | Results Table -- SI Units | null | PC_HFM_Wet_conductivity_210726_R2.tst:row 6 | null | fsri_hfm_si | separator-v32 | null | null | PC | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "Results Table -- SI Units", "source_file": "data/runs/2026-10-26_source_probe_fsri/raw/b6687789d92a123f97ef8442517d96981f19b38fe6e6740b90fb2e5ca95578de.tst", "source_sha256": "b6687789d92a123f97ef8442517d96981f19b3... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 45.01 | measurement | null | null | through-plane | TA Instruments FOX HFM; SI results | FSRI Wet; ambient/unconditioned Wet is not electrolyte soaking | null | measured | R2 | null | null | null | null | accepted | Instrument-reported results; repeated setpoints retained as rows, not independent experiments. | null | fsri:PC_HFM_Wet_conductivity_210726_R2.tst:si:6 | License/reuse permission not established; local research evidence only | 023059767a170e39f61e5314415a33b8ce4756a339150c617edbfa32675a672a | 1 | not_reported_in_linked_identity | |||||
69de63dc4ebda54631b9698363ddd51c734bdab56cb5952f2f06999620b0bca9 | 0dea6d581abd14726def4375f67162783f2cf13a7698bac96c0eda96f68e1fbb | patents | data/runs/2026-10-23_balanced/raw/ca3748f4f0a6f12d7edbdacd3123d9599826f0f0ae5f0bfb3990072474fa9dec.bin | ca3748f4f0a6f12d7edbdacd3123d9599826f0f0ae5f0bfb3990072474fa9dec | EP4040589A1:Ex.10 | tensile_strength | Tensile strength (kgf/cm 2 ) | 1250 | kgf/cm 2 | 122.583125 | MPa | https://patents.google.com/patent/EP4040589A1/en | null | table_3 | null | 11 | 7 | patent_html_table | separator-v32 | null | null | PE | inherited_recipe | [{"locator": "p0137", "text": "A polyethylene porous film (available from Toray, porosity: 45%) having a thickness of 9 µm was prepared as a polyolefin porous substrate."}, {"locator": "p0143", "text": "In this manner, a crosslinked separator for a lithium secondary battery comprising a crosslinked polyolefin porous su... | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h0037 | (6) Evaluation of Tensile Strength in Machine Direction and Transverse Direction and Change in Tensile Strength in Machine Direction A specimen having a size of 100 mm × 15 mm was prepared. According to ASTM D882, the specimen was drawn in each of the machine direction and the transverse direction at a rate of 50 mm/mi... | null | measured | null | null | null | {"offset": 0, "scale": 0.0980665} | null | accepted | Publication EP4040589A1; Ex.10; printed unit: kgf/cm 2 . Example identity and experimental protocol retained; no processing temperature inferred. | 75849009 | null | License/reuse permission not established; local research evidence only | 0233263d05f110fc12c02ca979908b88ccf0a4e5000e77a1e16a531c54c641d9 | 1 | not_reported_in_linked_identity | |||||
b1024dffe4cc8ba9546418ffcfe842286f133a8ac86b88f7f6965395f7af0678 | 897d6da7011d77063394482c1b28d47fa21c84bc9531cc1fc498cf4a55e23f00 | manual | data/runs/2026-10-30_source_property_probe/raw/ad2ad1fb7fb3cf2c96f1059f5c22deef717f93aa7ef3c26b3a4b4fccafed8deb.csv | ad2ad1fb7fb3cf2c96f1059f5c22deef717f93aa7ef3c26b3a4b4fccafed8deb | US10326120B2:Example 4 | thermal_expansion_strain | thermal_expansion_strain | 10.5 | % | 10.5 | % | https://patents.google.com/patent/US10326120B2/en | null | TABLE 1 | null | 10 | 5 | manual_structured_import | separator-v32 | null | null | PE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "TABLE 1", "source_file": "data/runs/2026-10-30_source_property_probe/raw/ad2ad1fb7fb3cf2c96f1059f5c22deef717f93aa7ef3c26b3a4b4fccafed8deb.csv", "source_sha256": "ad2ad1fb7fb3cf2c96f1059f5c22deef717f93aa7ef3c26b3a4b... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | null | separator_component | not_reported | null | null | null | reported | 105 | exposure | 30 | null | TD | Suspended without tension; oven 105 C for 30 min; post-treatment dimensional change | porous substrate before coating; finite dimensional strain, not differential thermal expansion coefficient | null | measured | null | null | null | null | null | accepted | Reviewed primary source data/runs/2026-10-19_expansion/raw/5a7806c9ed63c232a1162cb5abf9ebf04bdb5b17e34d68956ae71dcc0ca0f2b2.bin; SHA256 5a7806c9ed63c232a1162cb5abf9ebf04bdb5b17e34d68956ae71dcc0ca0f2b2. Header and test method reviewed in primary HTML. Negative values retained. Repeated Example 2 table row counted once. | null | null | Locally reviewed primary-source cells; source reuse terms apply. | 0240d0dbe7b6f38d8927257f03676a2486020836ca97ca05d453922e44660336 | 1 | not_reported_in_linked_identity | |||||
0dfb9d311e38dbd9ed7c870784762507fc7c87f96391dec7e3dfb243f94cddf2 | 9d15cd73afa94ce1a204e5a99a113bb6c419f1205ac759270e8222460c94ef60 | patents | data/runs/2026-10-26_balanced/raw/2a78626aa89e2d32a3ab95745666f209e7053579661cbb2d741e18b56d7c63f4.bin | 2a78626aa89e2d32a3ab95745666f209e7053579661cbb2d741e18b56d7c63f4 | EP2408043A1:Example 2-7 | melting_temperature | Melting point (°C) | 160 | °C | 160 | C | https://patents.google.com/patent/EP2408043A1/en | null | table_3 | null | 8 | 4 | patent_html_table | separator-v32 | null | null | null | sample_label_not_found | null | No complete sample-specific material recipe linked; document-wide mentions are insufficient | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | null | (1) Melting Point (°C) The melting point was measured with the DSC 60 manufactured by Shimadzu Corp. A sample (3 mg) was sampled and used as a measurement sample. The sample was spread over an aluminum open sample pan of 5 mm in diameter, and a cramping cover was placed thereon, and fixed in the pan with a sample seale... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0C"} | null | accepted | Publication EP2408043A1; Example 2-7; printed unit: °C. Example identity and experimental protocol retained; no processing temperature inferred. | 42728366 | null | License/reuse permission not established; local research evidence only | 0247c9e81a4c0dbb48894e8fe5fc9f0815e8997a87bd5ccf12ce4ef3c817b1ce | 1 | not_reported_in_linked_identity | |||||
eb61c1b40384190d2473383b148e7f4a01525be65296c22ff3b8c340482f0675 | 1211453927c908113d97002337e2485d761dc8d1d4f1a34eaaf834431364f413 | fsri | data/runs/2026-10-30_thermal/raw/2899d07a75f0d977f344e9c26ea5cd2e6070365b0a7452521a793048a7e099da.csv | 2899d07a75f0d977f344e9c26ea5cd2e6070365b0a7452521a793048a7e099da | LDPE_STA_N2_30KData_210908_R1 | sta_mass_percent | Mass(subtr.2)/% | 98.7866 | % | 98.7866 | % | https://raw.githubusercontent.com/ulfsri/fsri_materials_database/a432697e4b7d40f642b5cc8f384506439ebb32df/01_Data/LDPE/STA/N2/30K_min/LDPE_STA_N2_30KData_210908_R1.csv | null | null | null | LDPE_STA_N2_30KData_210908_R1.csv:CSV row 59 | Mass(subtr.2)/% | fsri_sta_native_csv | separator-v32 | null | null | LDPE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "LDPE_STA_N2_30KData_210908_R1.csv:CSV row 59", "source_file": "data/runs/2026-10-30_thermal/raw/2899d07a75f0d977f344e9c26ea5cd2e6070365b0a7452521a793048a7e099da.csv", "source_sha256": "2899d07a75f0d977f344e9c26ea5c... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | null | null | bulk polymer reference | bulk_reference | not_reported | null | null | null | reported | 54.977 | measurement | null | 30 | unspecified | NETZSCH STA 449F3; source-exported baseline-subtracted STA signal | N2 source directory; dynamic heating; source signal sign retained | null | measured | R1 | fsri:STA:LDPE_STA_N2_30KData_210908_R1 | null | null | null | accepted | Bulk polymer, not separator performance. Correlated samples of one curve, not independent experiments. Native source-exported row selected within 0.25 C of 5 C grid, 50–300 C; no further interpolation. Mass signals retain baseline offsets, not normalized mass loss. DSC is heat flow, not heat capacity. Metadata SHA256 8... | null | fsri:STA:LDPE_STA_N2_30KData_210908_R1:row:59:sta_mass_percent | License/reuse permission not established; local research evidence only | 02481fc07dfce2ef9b6f7190640ebb8e898bf3c972ef1559eba632bb2d9c81ee | 1 | LDPE | explicit_identity_or_reviewed_sample_evidence | [{"field": "polymer", "text": "LDPE", "labels": ["LDPE"]}, {"field": "sample_id", "text": "LDPE_STA_N2_30KData_210908_R1", "labels": ["LDPE"]}] | LDPE | ||
26ad836080cf44fb9019c2dd9697b31cd9186558e8db4d91152115faa94e33bb | 903aca71e375e64cc23a533e14b7f7d988ef48d030696fe23af39827cdc52d6a | manual | data/runs/2026-10-23_balanced_verified/raw/2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d704fa1.csv | 2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d704fa1 | PMC6804153:PE-PVDF Separator | puncture_force | puncture_force | 6.20 | N | 6.2 | N | https://www.ebi.ac.uk/europepmc/webservices/rest/PMC6804153/fullTextXML | null | materials-12-03125-t002 | null | 67 | 3 | manual_structured_import | separator-v32 | null | null | PE | supplied_source_identity | [{"basis": "Supplied source material field; see observation notes for primary-source review", "locator": "materials-12-03125-t002", "source_file": "data/runs/2026-10-23_balanced_verified/raw/2bc789f70330fe5404698791cc6a84f5aae39f76ac76a129fa3032720d704fa1.csv", "source_sha256": "2bc789f70330fe5404698791cc6a84f5aae39f76... | Material supplied by source adapter or reviewed import; see source coordinates and notes | null | PVDF organic particles | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Reviewed primary XML table/result; reported scalar only | null | null | measured | null | null | null | null | null | accepted | Primary XML SHA256 15a8bc8ba95334b0c7058529c6091d1ba242fcdfb5107008f225b29d1bebd467; XML row 4, column 3; printed cell 6.20; exact evidence: Puncture test (N) 5.67 6.20 | null | null | Reviewed primary XML table extracts; preserve exact source coordinates and hashes; original source reuse terms apply. | 0254bd1ba5fe6bbcae62c7e991cd7b396d15ad713542c507060643f8c3622f9f | 1 | not_reported_in_linked_identity | |||||
4f2c426534fefb19b553530acc7c54949f6bfe5731ef11c5c07471b9b2dc6790 | 0a43b06ff83c7df583a53deae871e37f727a313bef3fda6c2c7eaa42dfad1b27 | patents | data/raw/9de75e6d57412345350ac3f88d9f7776aacd512f7179cbf56243e5ba58f5d1cf.bin | 9de75e6d57412345350ac3f88d9f7776aacd512f7179cbf56243e5ba58f5d1cf | US20240222710A1:Comparative Ex. 3 | shutdown_temperature | Shutdown temperature (° C.) | 200 | ° C. | 200 | C | https://patents.google.com/patent/US20240222710A1/en | null | TABLE 1 | null | 19 | 7 | patent_html_table | separator-v32 | null | null | PI | explicit_recipe | [{"locator": "p-0293", "text": "A polyimide porous film (Guhyun Co., porosity: 45%) having a thickness of 16.3 m was used as a separator for a lithium secondary battery without any further treatment."}] | null | null | null | null | null | separator | not_reported | null | null | null | reported | null | unknown | null | null | unspecified | Patent experimental protocol h-0026 | (5) Evaluation of Shutdown Temperature After fixing the separator to an air permeability tester, the shutdown temperature was determined by measuring air permeability under heating at a rate for 5° C. per minute. Herein, the air permeability was determined by measuring a time (sec) required for 100 mL of air to pass th... | null | measured | null | null | null | {"canonical_unit": "C", "unit_alias": "\u00b0 C."} | null | accepted | Publication US20240222710A1; Comparative Ex. 3; printed unit: ° C.. Example identity and experimental protocol retained; no processing temperature inferred. | 83932843 | null | License/reuse permission not established; local research evidence only; Locally credential-redacted source; original acquisition SHA256 d07b7aa35cc933b67f6c084d752cb83e546db868724c39e924604458f4b3e49d; current SHA256 identifies sanitized bytes. | 0254f0c24ac1194194a2283af30fcecc269dce2a09d4c631b1c31c4edee0d4c0 | 1 | not_reported_in_linked_identity | |||||
1b7f947002faaeb526308aed33ec5f10be5827ebdcc599bc47b94a6501cbf29a | 1377fc49cc188be3568757283f01757ac545081b8454b408f060658736b9f1d6 | patents | data/runs/2026-10-19_expansion/raw/78fc83b885911a313b35805edc6a46500e6c3f29a8aeb5ca9a46ba9c8109181a.bin | 78fc83b885911a313b35805edc6a46500e6c3f29a8aeb5ca9a46ba9c8109181a | EP3181621A1:Comparative Example 1 | thermal_shrinkage | Shrinkage Shrinkage at 105°C in the MD (%) | 4.0 | % | 4 | % | https://patents.google.com/patent/EP3181621A1/en | null | table_2 | null | 10 | 5 | patent_html_table | separator-v32 | null | null | PE | reviewed_sample_link | [{"locator": "p0072", "text": "A polyethylene composition consisting of 30 wt.% of a PE 1 (ultrahigh molecular weight polyethylene, weight average molecular weight (Mw): 2.89 × 10 6 , molecular weight distribution (Mw/Mn): 5.28) as an ultrahigh molecular weight polyethylene and 70 wt.% of a PE2 (high-density polyolefin... | null | null | null | null | null | separator | not_reported | null | null | null | reported | 105 | exposure | 480 | null | MD | Patent experimental protocol h0018 | 6. Thermal shrinkage The shrinkage in the MD when the microporous membrane was held for 8 hours at 105°C was measured three times, and the average was used as the thermal shrinkage in the MD. In addition, similar measurements were taken in the TD to determine the thermal shrinkage in the TD. | null | measured | null | null | null | null | null | accepted | Publication EP3181621A1; Comparative Example 1; printed unit: %. Example identity and experimental protocol retained; no processing temperature inferred. Reviewed sample identity: p0072 | p0079 | 55304161 | null | License/reuse permission not established; local research evidence only | 0255bd65708949712595bac77dfa292c82c6e4459511efaafec0070073d00a1d | 2 | not_reported_in_linked_identity | UHMWPE |
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